Understanding Forage Palm Mucilage Behavior: Harnessing Plackett–Burman Screening for Tailoring Formulation and Process

The rheological and textural behavior of a highly viscous solution containing forage palm mucilage (FPM) was investigated using the Plackett–Burman (PB) design and multivariate analysis. The influence of carbohydrates (xanthan gum (XG), carboxymethyl cellulose (CMC), and sucrose), proteins (soy, egg, and whey), and salts (NaCl and CaCl2), as well as pH and temperature, on FPM formulations was evaluated (α < 0.10 and R2 > 0.75). The flow curves indicate that gels fitted to the Ostwald-de Waele model and presented pseudoplastic behavior. Apparent viscosity at 10 s−1 showed results between 0.05 and 36.16 Pa·s, affected by XG, FPM and egg albumin. Hysteresis (–1138 to 3950 Pa·s) was reduced with increasing pH (p = 0.041), indicating the formation of more stable three-dimensional networks. Significant effects on firmness (0.114–0.434 N), consistency (1.286–3.397 N·s), cohesiveness (0.047–0.167 N), and viscosity index (0.067–0.810 N·s) were observed for sucrose, salts, and temperature (p < 0.100). Chemometric analysis confirmed the influence of these factors on the evaluated responses but revealed no correlation between rheological and textural parameters.

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Journal
Polysaccharides
Published
2025-11-09
DOI
https://doi.org/10.3390/polysaccharides6040100
Primary Topic
Polysaccharides Composition and Applications
Type
article
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article

Understanding Forage Palm Mucilage Behavior: Harnessing Plackett–Burman Screening for Tailoring Formulation and Process

Sílvia Letícia Rivero Meza, María Teresa Pedrosa Silva Clerici, Giselle Pereira Cardoso, Marcio Masculino Schmiele et al.
Polysaccharides
Polysaccharides Composition and Applications
article

Understanding Forage Palm Mucilage Behavior: Harnessing Plackett–Burman Screening for Tailoring Formulation and Process

Sílvia Letícia Rivero Meza, María Teresa Pedrosa Silva Clerici, Giselle Pereira Cardoso, Marcio Masculino Schmiele, Tatiana Nunes Amaral, Irene Andressa, Vívian Machado Benassi, C. Roldan-Cruz, Nathália de Andrade Neves, MARIA LUIZA LAURINDO VIEIRA, P. M. de Oliveira, Monalisa Pereira Dutra Andrade, Larissa de Oliveira Ferreira Rocha, Sander Moreira Rodrigues, Tatiane Monteiro dos Santos, Kaliston Aurélio Lomba, Gabrielly de Fátima Rodrigues das Neves
article en

Abstract

The rheological and textural behavior of a highly viscous solution containing forage palm mucilage (FPM) was investigated using the Plackett–Burman (PB) design and multivariate analysis. The influence of carbohydrates (xanthan gum (XG), carboxymethyl cellulose (CMC), and sucrose), proteins (soy, egg, and whey), and salts (NaCl and CaCl2), as well as pH and temperature, on FPM formulations was evaluated (α < 0.10 and R2 > 0.75). The flow curves indicate that gels fitted to the Ostwald-de Waele model and presented pseudoplastic behavior. Apparent viscosity at 10 s−1 showed results between 0.05 and 36.16 Pa·s, affected by XG, FPM and egg albumin. Hysteresis (–1138 to 3950 Pa·s) was reduced with increasing pH (p = 0.041), indicating the formation of more stable three-dimensional networks. Significant effects on firmness (0.114–0.434 N), consistency (1.286–3.397 N·s), cohesiveness (0.047–0.167 N), and viscosity index (0.067–0.810 N·s) were observed for sucrose, salts, and temperature (p < 0.100). Chemometric analysis confirmed the influence of these factors on the evaluated responses but revealed no correlation between rheological and textural parameters.

PolysaccharidesVol. 6(4)
Universidade Federal de Viçosa (BR), Universidad Veracruzana (MX), Universidade Federal de Pelotas (BR), Universidade Estadual de Campinas (UNICAMP) (BR), Universidade Federal dos Vales do Jequitinhonha e Mucuri (BR), Universidad de las Naciones (MX), Instituto Tecnológico de Veracruz (MX)
Openalex Percentile: Top 61%
Polysaccharides Composition and Applications
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