Encapsulation of Allyl Isothiocyanate by Freeze- and Spray-Drying: Effects on Retention and Sensory Perception in Sodium-Reduced Soups

Allyl isothiocyanate (AITC) has been shown to enhance perceived saltiness in food products; however, it is also associated with a pungent and spicy flavour. The objective of this study was to assess the encapsulation of AITC with maltodextrin (MD) and gum Arabic (GA) using spray-drying (SD) and freeze-drying (FD) techniques, with and without the addition of a surfactant. Furthermore, the different encapsulated formulations were evaluated for their impact on sensory properties when added to soups. In total, twelve different treatments were investigated. The physicochemical characteristics (i.e., encapsulation efficiency, surface oil content, capsule morphology, and moisture content) and sensory properties (i.e., hedonic scales and rate-all-that-apply) of the encapsulated AITC particles were analyzed. Gas chromatography revealed low AITC retention in all FD formulations, while SD formulations with surfactants achieved up to 136.71 mg AITC/g powder. Sensory trials were conducted on eight formulations added to tomato soup (0.500 mg AITC/100 mL) (SD trial: <i>n</i> = 79, and FD trial: <i>n</i> = 93). FD resulted in relatively low AITC retention (with and without surfactants), while SD with surfactants led to higher AITC retention. None of the formulations significantly impacted the saltiness perception of the soups. FD soups significantly enhanced thickness, creaminess, and tomato flavour, increasing overall liking. This is the first study to evaluate the sensory properties and cross-modal interactions of encapsulated AITC. Further studies are needed to continue exploring the sensory properties, its release behaviour, overall stability, and shelf life of encapsulated AITC.

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Publication Details

Journal
Foods
Published
2025-11-07
DOI
https://doi.org/10.3390/foods14223810
Primary Topic
Microencapsulation and Drying Processes
Type
article
Field-Weighted Citation Impact
0.00

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article

Encapsulation of Allyl Isothiocyanate by Freeze- and Spray-Drying: Effects on Retention and Sensory Perception in Sodium-Reduced Soups

Matthew B. McSweeney, Nicoletta Faraone, Emily Dolan
Foods
Microencapsulation and Drying Processes
article

Encapsulation of Allyl Isothiocyanate by Freeze- and Spray-Drying: Effects on Retention and Sensory Perception in Sodium-Reduced Soups

Matthew B. McSweeney, Nicoletta Faraone, Emily Dolan
article en

Abstract

Allyl isothiocyanate (AITC) has been shown to enhance perceived saltiness in food products; however, it is also associated with a pungent and spicy flavour. The objective of this study was to assess the encapsulation of AITC with maltodextrin (MD) and gum Arabic (GA) using spray-drying (SD) and freeze-drying (FD) techniques, with and without the addition of a surfactant. Furthermore, the different encapsulated formulations were evaluated for their impact on sensory properties when added to soups. In total, twelve different treatments were investigated. The physicochemical characteristics (i.e., encapsulation efficiency, surface oil content, capsule morphology, and moisture content) and sensory properties (i.e., hedonic scales and rate-all-that-apply) of the encapsulated AITC particles were analyzed. Gas chromatography revealed low AITC retention in all FD formulations, while SD formulations with surfactants achieved up to 136.71 mg AITC/g powder. Sensory trials were conducted on eight formulations added to tomato soup (0.500 mg AITC/100 mL) (SD trial: <i>n</i> = 79, and FD trial: <i>n</i> = 93). FD resulted in relatively low AITC retention (with and without surfactants), while SD with surfactants led to higher AITC retention. None of the formulations significantly impacted the saltiness perception of the soups. FD soups significantly enhanced thickness, creaminess, and tomato flavour, increasing overall liking. This is the first study to evaluate the sensory properties and cross-modal interactions of encapsulated AITC. Further studies are needed to continue exploring the sensory properties, its release behaviour, overall stability, and shelf life of encapsulated AITC.

FoodsVol. 14(22)
Acadia University (CA)
Natural Sciences and Engineering Research Council of Canada
Openalex Percentile: Top 61%
Microencapsulation and Drying Processes
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