Laboratory Evaluation of the Physicochemical Properties of Novel Pre‐Mixed Putty‐Type Bioceramic Materials

This study aimed to compare the physicochemical properties of EndoSequence Root Repair Material (ERRM) Fast and CeraPutty with ProRoot MTA and Biodentine, focusing on setting time, radiopacity, microhardness, and pH. Setting time was measured using a Gilmore-type indenter applied every 5 min until no indentation was observed (n = 15 per group). Radiopacity was assessed via aluminium step wedge, microhardness using Vickers hardness, and pH changes with a digital pH meter. Nonparametric statistical analyses were conducted with a significance level of 95%. Biodentine exhibited the shortest setting time and highest microhardness, while ERRM Fast showed the highest radiopacity. High alkaline pH values were measured for all materials. Within the limitations of this study, the new pre-mixed calcium silicate materials exhibited physicochemical properties comparable to traditionally mixed materials, indicating their potential suitability for endodontic treatments. However, careful selection based on clinical requirements, including handling, setting time, and mechanical properties, is essential.

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Publication Details

Journal
Australian Endodontic Journal
Published
2025-10-29
DOI
https://doi.org/10.1111/aej.70031
Primary Topic
Endodontics and Root Canal Treatments
Type
article
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article

Laboratory Evaluation of the Physicochemical Properties of Novel Pre‐Mixed Putty‐Type Bioceramic Materials

Sang Won Kwak, Hyeon‐Cheol Kim, Minju Song, So‐Mang Lee
Australian Endodontic Journal
Endodontics and Root Canal Treatments
article

Laboratory Evaluation of the Physicochemical Properties of Novel Pre‐Mixed Putty‐Type Bioceramic Materials

Sang Won Kwak, Hyeon‐Cheol Kim, Minju Song, So‐Mang Lee
article en

Abstract

This study aimed to compare the physicochemical properties of EndoSequence Root Repair Material (ERRM) Fast and CeraPutty with ProRoot MTA and Biodentine, focusing on setting time, radiopacity, microhardness, and pH. Setting time was measured using a Gilmore-type indenter applied every 5 min until no indentation was observed (n = 15 per group). Radiopacity was assessed via aluminium step wedge, microhardness using Vickers hardness, and pH changes with a digital pH meter. Nonparametric statistical analyses were conducted with a significance level of 95%. Biodentine exhibited the shortest setting time and highest microhardness, while ERRM Fast showed the highest radiopacity. High alkaline pH values were measured for all materials. Within the limitations of this study, the new pre-mixed calcium silicate materials exhibited physicochemical properties comparable to traditionally mixed materials, indicating their potential suitability for endodontic treatments. However, careful selection based on clinical requirements, including handling, setting time, and mechanical properties, is essential.

Australian Endodontic Journal
National Health Insurance Service Ilsan Hospital (KR), Pusan National University Dental Hospital (KR), National Health Insurance Service (KR), Pusan National University (KR)
Openalex Percentile: Top 57%
Endodontics and Root Canal Treatments
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Laboratory Evaluation of the Physicochemical Properties of Novel Pre‐Mixed Putty‐Type Bioceramic Materials — Sang Won Kwak, Hyeon‐Cheol Kim, et al. · Australian Endodontic Journal (2025) | TGRS Research Map | TGRS