High-Throughput Robotic GIWAXS at ALS SAXS/WAXS Beamline

We present the development of a high-throughput, robotic GIWAXS platform for automated thin-film characterization at the ALS SAXS/WAXS beamline. The system features a UR5e robotic arm, a helium-purged sample chamber, integrated beamline data acquisition routines, and a web-based interface for sample tracking. Designed for seamless compatibility with computational workflows, the control software enables real-time data transfer, analysis, and autonomous experimentation, greatly increasing throughput with additional gains in noise reduction and resource management. The platform also supports future integration with synthesis and sample-processing systems, such as Sciprios and North Robotics, paving the way for closed-loop, data-driven materials research and establishing a means to accelerate the pace of materials innovation.

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Publication Details

Journal
Photon Science
Published
2025-10-22
DOI
https://doi.org/10.1021/photonsci.5c00017
Citations
2
Primary Topic
Particle Detector Development and Performance
Type
article
Field-Weighted Citation Impact
3.74
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High-Throughput Robotic GIWAXS at ALS SAXS/WAXS Beamline

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2 citations
Photon Science
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High-Throughput Robotic GIWAXS at ALS SAXS/WAXS Beamline

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article en
2 citations

Abstract

We present the development of a high-throughput, robotic GIWAXS platform for automated thin-film characterization at the ALS SAXS/WAXS beamline. The system features a UR5e robotic arm, a helium-purged sample chamber, integrated beamline data acquisition routines, and a web-based interface for sample tracking. Designed for seamless compatibility with computational workflows, the control software enables real-time data transfer, analysis, and autonomous experimentation, greatly increasing throughput with additional gains in noise reduction and resource management. The platform also supports future integration with synthesis and sample-processing systems, such as Sciprios and North Robotics, paving the way for closed-loop, data-driven materials research and establishing a means to accelerate the pace of materials innovation.

Photon ScienceVol. 1(1)
Lawrence Berkeley National Laboratory (US), Advanced Light Source, University of Southern Mississippi (US)
Openalex Percentile: Top 7%
Particle Detector Development and Performance
3.74
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