Shear Bond Strength of CAD/CAM Highly Translucent Zirconia Bonded to Occlusal Dentin after Different Extrinsic Modifications: An In vitro Study

Introduction The bond between highly translucent zirconia (HTZ) onlay restorations and the resin cement is challenging due to its non-glassy structure. This study compares the effect of different extrinsic modifications on the shear bond strength of HTZ to occlusal dentin after thermocycling. Methods Forty human molars were prepared and stored in 0.5% chloramine. Ceramic discs (n = 40) were distributed into four groups. HTZ discs underwent airborne-particle abrasion (Group ZA), 30 μm diamond abrasion (Group ZB), and no treatment (Group ZN). All HTZ discs were treated with 10-MDP primer. Lithium disilicate discs (Group LD-control) were treated with about 4.5% hydrofluoric acid and silane. All discs were cemented to dentin using resin cement. SBS was measured using a universal testing machine, and fracture types were assessed. Results Group ZA showed the greatest SBS among HTZ groups (Tukey’s test; p < 0.05), though none exceeded the LD-control group ( p < 0.0001). Most fractures occurred at the zirconia-resin cement interface, relatively less in group ZA (40%). Discussion The current study highlights that combined mechanical and chemical treatment has the potential to strengthen the bond of HTZ to occlusal dentin. Moreover, it includes both the resin-zirconia and resin-dentin interfaces in the experiment that closely simulates the intracoronal restoration. One of the limitations is that the results may vary in the oral environment during the clinical trials because of external factors, such as saliva, food, and masticatory forces. Use of thermo-mechanical ageing could have overcome this limitation. Conclusion Combined mechanical and chemical treatment improved HTZ bonding to dentin. Further clinical studies are needed to establish optimal surface modification protocols.

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Publication Details

Journal
The Open Dentistry Journal
Published
2025-09-16
DOI
https://doi.org/10.2174/0118742106418713250914060125
Primary Topic
Dental materials and restorations
Type
article
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Shear Bond Strength of CAD/CAM Highly Translucent Zirconia Bonded to Occlusal Dentin after Different Extrinsic Modifications: An In vitro Study

Mohammed M. Al Moaleem, Thilla Sekar Vinothkumar, Mohmed Isaqali Karobari, Syed Nahid Basheer et al.
The Open Dentistry Journal
Dental materials and restorations
article

Shear Bond Strength of CAD/CAM Highly Translucent Zirconia Bonded to Occlusal Dentin after Different Extrinsic Modifications: An In vitro Study

Mohammed M. Al Moaleem, Thilla Sekar Vinothkumar, Mohmed Isaqali Karobari, Syed Nahid Basheer, Wasan Hassan Hamzi, Amal Ali Yaqoub, Nasreen Hassan Albar, Halima Faya Almashy
article en

Abstract

Introduction The bond between highly translucent zirconia (HTZ) onlay restorations and the resin cement is challenging due to its non-glassy structure. This study compares the effect of different extrinsic modifications on the shear bond strength of HTZ to occlusal dentin after thermocycling. Methods Forty human molars were prepared and stored in 0.5% chloramine. Ceramic discs (n = 40) were distributed into four groups. HTZ discs underwent airborne-particle abrasion (Group ZA), 30 μm diamond abrasion (Group ZB), and no treatment (Group ZN). All HTZ discs were treated with 10-MDP primer. Lithium disilicate discs (Group LD-control) were treated with about 4.5% hydrofluoric acid and silane. All discs were cemented to dentin using resin cement. SBS was measured using a universal testing machine, and fracture types were assessed. Results Group ZA showed the greatest SBS among HTZ groups (Tukey’s test; p < 0.05), though none exceeded the LD-control group ( p < 0.0001). Most fractures occurred at the zirconia-resin cement interface, relatively less in group ZA (40%). Discussion The current study highlights that combined mechanical and chemical treatment has the potential to strengthen the bond of HTZ to occlusal dentin. Moreover, it includes both the resin-zirconia and resin-dentin interfaces in the experiment that closely simulates the intracoronal restoration. One of the limitations is that the results may vary in the oral environment during the clinical trials because of external factors, such as saliva, food, and masticatory forces. Use of thermo-mechanical ageing could have overcome this limitation. Conclusion Combined mechanical and chemical treatment improved HTZ bonding to dentin. Further clinical studies are needed to establish optimal surface modification protocols.

The Open Dentistry JournalVol. 19(1)
Openalex Percentile: Top 70%
Dental materials and restorations
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