Synergistic Effects of Temperature and Cooling Rate on Lamellar Microstructure Evolution and Mechanical Performance in Ti-44.9Al-4.1Nb-1.0Mo-0.1B-0.05Y-0.05Si Alloy
TiAl alloys are ideal candidates to replace nickel-based superalloys in aero-engines due to their low density and high specific strength, yet their industrial application is hindered by narrow heat treatment windows and unbalanced mechanical performance. To address this, this study investigates the microstructure and mechanical properties of Ti-44.9Al-4.1Nb-1.0Mo-0.1B-0.05Y-0.05Si (TNM-derived) alloys hot-rolled in the (α<sub>2</sub> + γ) two-phase region. The research employs varying heat treatment temperatures (1150-1280 °C) and cooling rates (0.1-2.5 °C/s), combined with XRD, SEM, EBSD characterization, and 800 °C high-temperature tensile tests. Key findings: Discontinuous dynamic recrystallization (DDRX) of γ grains is the primary mechanism refining lamellar colonies during deformation. Higher heat treatment temperatures reduce γ/β phases (which constrain colony growth), increasing the volume fraction of lamellar colonies but exerting minimal impact on interlamellar spacing. Faster cooling shifts γ lamella nucleation from confined to grain boundaries to multi-sites (grain boundaries, γ lamella peripheries, α grains) and changes grain boundaries from jagged and interlocking to smooth and straight, which boosts nucleation sites and refines interlamellar spacing. Fine lamellar colonies and narrow interlamellar spacing enhance tensile strength, while eliminating brittle βo phases and promoting interlocking boundaries with uniform equiaxed γ grains improve plasticity.
Authors
- Kashif Naseem (ORCID: https://orcid.org/0009-0000-2384-0975)
- Shiwei Tian (ORCID: https://orcid.org/0000-0002-7135-4768)
- Fengliang Tan (ORCID: https://orcid.org/0000-0001-9438-4743)
- Ning Liu (ORCID: https://orcid.org/0000-0002-6498-6118)
- Yantao Li (ORCID: https://orcid.org/0000-0001-5943-3503)
- Zhichao Zhu (ORCID: https://orcid.org/0000-0003-3565-6344)
- Jinbiao Cui
Institutions
- Hunan University of Humanities, Science and Technology (CN)
- Shandong Iron and Steel Group (China) (CN)
- University of Science and Technology Beijing (CN)
Publication Details
- Journal
- Materials
- Published
- 2025-10-09
- DOI
- https://doi.org/10.3390/ma18194641
- Primary Topic
- Intermetallics and Advanced Alloy Properties
- Type
- article
- Field-Weighted Citation Impact
- 0.00
Funders
- National Natural Science Foundation of China
- Natural Science Foundation of Hunan Province