Tailoring solidification and strength enhancement through process parameter optimization in Nb-added 316L stainless steel fabricated by directed energy deposition (DED)

Additive manufacturing (AM), particularly the directed energy deposition (DED) process, enables the fabrication of metallic components with complex geometries and is widely applied across high-value industries. However, the microstructure and mechanical properties of DED-fabricated parts are highly sensitive to processing parameters, making consistent quality control challenging. In this study, 316L stainless steel with 2 wt.% Nb addition was fabricated under systematically varied scan speeds and laser powers to clarify the process–microstructure–property relationships unique to Nb-modified alloys. Results showed that increasing scan speed reduced the melt pool size and promoted a solidification mode transition from dendritic to cellular morphologies. Because dendritic structures provided higher hardness and strength through stronger Nb segregation at dendrite boundaries, the cellular-dominated condition at 1.2 m/min exhibited the lowest mechanical performance. Increasing laser power reduced the cooling rate and led to coarsening of the solidification structure, which further degraded strength. Notably, under rapid cooling conditions, Nb segregation suppressed nucleation and promoted ab-normal growth of the solidification structure, resulting in behavior distinct from conventional 316L stainless steel where refinement is expected. These findings demonstrate that process optimization windows established for conventional 316L cannot be directly ap-plied to Nb-modified alloys. Instead, alloy-specific segregation behavior must be incorporated into parameter optimization strategies to achieve reliable microstructure and mechanical properties in DED-fabricated Nb-added stainless steels.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-10-10
DOI
https://doi.org/10.1016/j.jmrt.2025.10.082
Citations
2
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
1.43
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article

Tailoring solidification and strength enhancement through process parameter optimization in Nb-added 316L stainless steel fabricated by directed energy deposition (DED)

Hyejin Song, Sung Hyuk Park, Soo Bin Han, Ho‐Jin Lee et al.
2 citations
Journal of Materials Research and Technology
Additive Manufacturing Materials and Processes
1.43
article

Tailoring solidification and strength enhancement through process parameter optimization in Nb-added 316L stainless steel fabricated by directed energy deposition (DED)

Hyejin Song, Sung Hyuk Park, Soo Bin Han, Ho‐Jin Lee, Jin Seok Jang, Yoori Lee
article en
2 citations

Abstract

Additive manufacturing (AM), particularly the directed energy deposition (DED) process, enables the fabrication of metallic components with complex geometries and is widely applied across high-value industries. However, the microstructure and mechanical properties of DED-fabricated parts are highly sensitive to processing parameters, making consistent quality control challenging. In this study, 316L stainless steel with 2 wt.% Nb addition was fabricated under systematically varied scan speeds and laser powers to clarify the process–microstructure–property relationships unique to Nb-modified alloys. Results showed that increasing scan speed reduced the melt pool size and promoted a solidification mode transition from dendritic to cellular morphologies. Because dendritic structures provided higher hardness and strength through stronger Nb segregation at dendrite boundaries, the cellular-dominated condition at 1.2 m/min exhibited the lowest mechanical performance. Increasing laser power reduced the cooling rate and led to coarsening of the solidification structure, which further degraded strength. Notably, under rapid cooling conditions, Nb segregation suppressed nucleation and promoted ab-normal growth of the solidification structure, resulting in behavior distinct from conventional 316L stainless steel where refinement is expected. These findings demonstrate that process optimization windows established for conventional 316L cannot be directly ap-plied to Nb-modified alloys. Instead, alloy-specific segregation behavior must be incorporated into parameter optimization strategies to achieve reliable microstructure and mechanical properties in DED-fabricated Nb-added stainless steels.

Journal of Materials Research and TechnologyVol. 39
Kyungpook National University (KR), Korea Evaluation Institute of Industrial Technology (KR)
Openalex Percentile: Top 17%
Additive Manufacturing Materials and Processes
1.43
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