Effect of aging treatment on microstructure, mechanical properties and corrosion behavior of AZ91 / 64SiO <sub>2</sub> -31CaO-5P <sub>2</sub> O <sub>5</sub> composite

This study explores the microstructural evolution and corrosion resistance of AZ91 magnesium alloy composites reinforced with bioactive glass (BG) particles and processed via friction stir extrusion (FSE), followed by aging heat treatment. The severe plastic deformation induced by FSE transforms the as-cast structure into a refined, equiaxed grain morphology, while subsequent aging promotes the controlled precipitation of β-Mg 17 Al 12 phases. BG particles acting as nucleation sites for precipitates and inhibiting grain coarsening during thermal exposure. These combined effects lead to significant improvements in mechanical performance (yield strength of 285.1 MPa and a hardness of 81.9 HV). Electrochemical analyses indicate that both aging and BG reinforcement enhance corrosion resistance by facilitating the formation of protective surface films and reducing cathodic reaction kinetics.

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Publication Details

Journal
Materials Science and Technology
Published
2025-10-03
DOI
https://doi.org/10.1177/02670836251376465
Primary Topic
Magnesium Alloys: Properties and Applications
Type
article
Field-Weighted Citation Impact
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article

Effect of aging treatment on microstructure, mechanical properties and corrosion behavior of AZ91 / 64SiO 2 -31CaO-5P 2 O 5 composite

Sayed Mahmood Rabiee, Hamed Jamshidi Aval, Pourya Motavallian
Materials Science and Technology
Magnesium Alloys: Properties and Applications
article

Effect of aging treatment on microstructure, mechanical properties and corrosion behavior of AZ91 / 64SiO 2 -31CaO-5P 2 O 5 composite

Sayed Mahmood Rabiee, Hamed Jamshidi Aval, Pourya Motavallian
article en

Abstract

This study explores the microstructural evolution and corrosion resistance of AZ91 magnesium alloy composites reinforced with bioactive glass (BG) particles and processed via friction stir extrusion (FSE), followed by aging heat treatment. The severe plastic deformation induced by FSE transforms the as-cast structure into a refined, equiaxed grain morphology, while subsequent aging promotes the controlled precipitation of β-Mg 17 Al 12 phases. BG particles acting as nucleation sites for precipitates and inhibiting grain coarsening during thermal exposure. These combined effects lead to significant improvements in mechanical performance (yield strength of 285.1 MPa and a hardness of 81.9 HV). Electrochemical analyses indicate that both aging and BG reinforcement enhance corrosion resistance by facilitating the formation of protective surface films and reducing cathodic reaction kinetics.

Materials Science and Technology
Babol Noshirvani University of Technology (IR)
Openalex Percentile: Top 82%
Magnesium Alloys: Properties and Applications
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