Experimental Study on the Time Response of the Microstructure of a Bentonite Suspension

To obtain deeper information on the role played by microstructure evolution with time of particle suspensions specifically used in drilling processes, two representative time scales of a bentonite suspension were proposed. On one hand, a thixotropic time, which represents how fast the microstructure of the suspensions reaches equilibrium between build-up and break-down under shear, was obtained from hysteresis loop tests. On the other hand, a representative relaxation time, which refers to the time it takes to dissipate the stresses developed in the microstructure returning to the original free-stress state after some disturbance of the microstructure, was obtained from frequency sweep tests in the linear viscoelastic region using the Generalized Maxwell Model. The ratio of the relaxation time to the thixotropic time, named the thixo-elastic parameter, was lower than unity. Therefore, bentonite suspensions reach an equilibrium state resulting from equality of break and build processes after a long time of rest, while returning very fast to their original free-stress state, enabling the microstructure to rebuild mainly through a thixotropic phenomenon, which was almost not affected by internal stresses, and which facilitates the entrapping of rock cuttings generated during drilling processes.