High-Temperature Oxidation Behavior of an Additively Manufactured Alumina-Forming Austenitic Stainless Steel

High-temperature oxidation behavior of an alumina-forming austenitic stainless steel (AFA25) produced by additive manufacturing (AM) has been studied at 850 °C in air and compared to the conventional wrought alloy. The mass gain measurements during high-temperature oxidation tests were performed to understand the rate of oxidation, oxidation characteristics, and morphology of oxides that form in these alloys. X-ray diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy were used to characterize the microstructure and oxide scale formation during high-temperature exposure. A similar alumina scale was observed on both wrought and AM alloys. The continuous alumina layer that forms in these alloys provides superior oxidation resistance. This paper shows that a variation in AM build parameters influences the oxidation properties, where one AM alloy with a lower laser power to hatch ratio depicts much better oxidation properties compared to conventional wrought AFA alloys.

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Publication Details

Journal
Corrosion and Materials Degradation
Published
2025-09-26
DOI
https://doi.org/10.3390/cmd6040047
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
0.00

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article

High-Temperature Oxidation Behavior of an Additively Manufactured Alumina-Forming Austenitic Stainless Steel

Rajeev Gupta, Amit Pandey, A. Chatterjee, Sedigheh Rashidi
Corrosion and Materials Degradation
Additive Manufacturing Materials and Processes
article

High-Temperature Oxidation Behavior of an Additively Manufactured Alumina-Forming Austenitic Stainless Steel

Rajeev Gupta, Amit Pandey, A. Chatterjee, Sedigheh Rashidi
article en

Abstract

High-temperature oxidation behavior of an alumina-forming austenitic stainless steel (AFA25) produced by additive manufacturing (AM) has been studied at 850 °C in air and compared to the conventional wrought alloy. The mass gain measurements during high-temperature oxidation tests were performed to understand the rate of oxidation, oxidation characteristics, and morphology of oxides that form in these alloys. X-ray diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy were used to characterize the microstructure and oxide scale formation during high-temperature exposure. A similar alumina scale was observed on both wrought and AM alloys. The continuous alumina layer that forms in these alloys provides superior oxidation resistance. This paper shows that a variation in AM build parameters influences the oxidation properties, where one AM alloy with a lower laser power to hatch ratio depicts much better oxidation properties compared to conventional wrought AFA alloys.

Corrosion and Materials DegradationVol. 6(4)
University of Akron (US), North Carolina State University (US)
U.S. Department of Energy
Openalex Percentile: Top 73%
Additive Manufacturing Materials and Processes
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