Investigation of texture evolution and multi-mechanism strengthening in NiTi alloy produced via selective laser melting

The mechanical performance of NiTi alloys is strongly governed by microstructural features such as densification, grain morphology, and dislocation density. However, quantitative insights into how processing parameters systematically control grain size, high-angle grain boundary (HAGB) fraction, texture characteristics, and kernel average misorientation (KAM) to achieve targeted property tuning remain limited. This study integrates experimental analysis, thermo-fluid coupling simulations, and theoretical modeling to systematically investigate the effects of laser power (100–140 W) and scanning speed (900–1100 mm/s) on the densification behavior and microstructural evolution of NiTi alloys fabricated by selective laser melting (SLM). The simulations reveal the evolution of Marangoni convection within the melt pool under varying energy densities, while metallographic analysis quantifies the correlation between porosity and processing parameters. The optimal process parameters (130 W, 1000 mm/s) yielded a tensile strength of 549 MPa, elongation of 6.39 %, elastic modulus of 21.04 GPa, and microhardness of 316–321 HV. EBSD analysis showed HAGB fractions of 41.7 % (X–Z) and 41.4 % (X–Y), with average grain sizes of 19.03 μm and 27.44 μm. TEM revealed abundant linear dislocations and uniformly dispersed NiTi 2 precipitates. These results demonstrate that the combination of high densification, strong texture, and multiple strengthening mechanisms enables a favorable balance of strength and ductility, thereby providing both theoretical guidance and practical insights for optimizing SLM-processed NiTi alloys.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-09-24
DOI
https://doi.org/10.1016/j.jmrt.2025.09.216
Citations
3
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
2.14
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article

Investigation of texture evolution and multi-mechanism strengthening in NiTi alloy produced via selective laser melting

Qingmao Zhang, Miaoning Yan, Yi Ba, Liang Guo et al.
3 citations
Journal of Materials Research and Technology
Additive Manufacturing Materials and Processes
2.14
article

Investigation of texture evolution and multi-mechanism strengthening in NiTi alloy produced via selective laser melting

Qingmao Zhang, Miaoning Yan, Yi Ba, Liang Guo, Jiaxing Guo
article en
3 citations

Abstract

The mechanical performance of NiTi alloys is strongly governed by microstructural features such as densification, grain morphology, and dislocation density. However, quantitative insights into how processing parameters systematically control grain size, high-angle grain boundary (HAGB) fraction, texture characteristics, and kernel average misorientation (KAM) to achieve targeted property tuning remain limited. This study integrates experimental analysis, thermo-fluid coupling simulations, and theoretical modeling to systematically investigate the effects of laser power (100–140 W) and scanning speed (900–1100 mm/s) on the densification behavior and microstructural evolution of NiTi alloys fabricated by selective laser melting (SLM). The simulations reveal the evolution of Marangoni convection within the melt pool under varying energy densities, while metallographic analysis quantifies the correlation between porosity and processing parameters. The optimal process parameters (130 W, 1000 mm/s) yielded a tensile strength of 549 MPa, elongation of 6.39 %, elastic modulus of 21.04 GPa, and microhardness of 316–321 HV. EBSD analysis showed HAGB fractions of 41.7 % (X–Z) and 41.4 % (X–Y), with average grain sizes of 19.03 μm and 27.44 μm. TEM revealed abundant linear dislocations and uniformly dispersed NiTi 2 precipitates. These results demonstrate that the combination of high densification, strong texture, and multiple strengthening mechanisms enables a favorable balance of strength and ductility, thereby providing both theoretical guidance and practical insights for optimizing SLM-processed NiTi alloys.

Journal of Materials Research and TechnologyVol. 39
South China Normal University (CN), Koito Manufacturing (Japan) (JP), South China University of Technology (CN)
Openalex Percentile: Top 12%
Additive Manufacturing Materials and Processes
2.14
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