Thioether Synthesis via the Nickel‐Catalyzed Electrochemical Cross Electrophile Coupling of Aryl/Alkyl Disulfides and Aryl/Alkyl Halides

A formal cross‐electrophile coupling approach enables the base‐free synthesis of (un)symmetric (hetero)aryl and alkyl sulfides from organic halides and disulfides. This water and air‐tolerant process utilizes the addition of electrochemically generated thiolate to an in situ‐generated reactive nickel species.

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Publication Details

Journal
Advanced Synthesis & Catalysis
Published
2025-09-19
DOI
https://doi.org/10.1002/adsc.70116
Primary Topic
Sulfur-Based Synthesis Techniques
Type
article
Field-Weighted Citation Impact
0.00
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article

Thioether Synthesis via the Nickel‐Catalyzed Electrochemical Cross Electrophile Coupling of Aryl/Alkyl Disulfides and Aryl/Alkyl Halides

Jona Queder, Gerhard Hilt
Advanced Synthesis & Catalysis
Sulfur-Based Synthesis Techniques
article

Thioether Synthesis via the Nickel‐Catalyzed Electrochemical Cross Electrophile Coupling of Aryl/Alkyl Disulfides and Aryl/Alkyl Halides

Jona Queder, Gerhard Hilt
article en

Abstract

A formal cross‐electrophile coupling approach enables the base‐free synthesis of (un)symmetric (hetero)aryl and alkyl sulfides from organic halides and disulfides. This water and air‐tolerant process utilizes the addition of electrochemically generated thiolate to an in situ‐generated reactive nickel species.

Advanced Synthesis & CatalysisVol. 367(22)
Carl von Ossietzky Universität Oldenburg (DE)
Openalex Percentile: Top 81%
Sulfur-Based Synthesis Techniques
DOIOpen Access PDFOpenAlex
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Thioether Synthesis via the Nickel‐Catalyzed Electrochemical Cross Electrophile Coupling of Aryl/Alkyl Disulfides and Aryl/Alkyl Halides — Jona Queder, Gerhard Hilt · Advanced Synthesis & Catalysis (2025) | TGRS Research Map | TGRS