Methodology for accounting of background in a neutron experiment with a 2D position-sensitive detector

A methodology for measuring and taking into account the background in a neutron single-crystal experiment with a position-sensitive detector is proposed. This methodology makes it possible to increase the ratio of integrated intensities to the standard deviation I/σ(I) for the diffraction reflection intensities and include in the array of experimental data the weak reflections that previously did not meet the condition I/σ(I)>3, and were not taken into account in crystallographic calculations. The methodology was tested on experimental data during structural studies of a Cs4(HSO4)3(H2PO4) crystals on the MOND diffractometer at the IR-8 reactor of the National Research Center “Kurchatov Institute”.

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Publication Details

Journal
Кристаллография / Crystallography Reports
Published
2025-01-01
DOI
https://doi.org/10.7868/s3034551025030017
Primary Topic
Nuclear Physics and Applications
Type
article
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article

Methodology for accounting of background in a neutron experiment with a 2D position-sensitive detector

N. N. Isakova
Кристаллография / Crystallography Reports
Nuclear Physics and Applications
article

Methodology for accounting of background in a neutron experiment with a 2D position-sensitive detector

N. N. Isakova
article en

Abstract

A methodology for measuring and taking into account the background in a neutron single-crystal experiment with a position-sensitive detector is proposed. This methodology makes it possible to increase the ratio of integrated intensities to the standard deviation I/σ(I) for the diffraction reflection intensities and include in the array of experimental data the weak reflections that previously did not meet the condition I/σ(I)>3, and were not taken into account in crystallographic calculations. The methodology was tested on experimental data during structural studies of a Cs4(HSO4)3(H2PO4) crystals on the MOND diffractometer at the IR-8 reactor of the National Research Center “Kurchatov Institute”.

Кристаллография / Crystallography ReportsVol. 70(3)
Openalex Percentile: Top 67%
Nuclear Physics and Applications
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