Unusual texture evolution in extruded AZ31 Mg alloy plates with bimodal grain structures

• The microstructural evolution of AZ31 alloy plates during various extrusion processes is analyzed. • The AZ31 Mg alloy plates, extruded via conventional methods under varying temperatures and speeds, exhibit bimodal grain structures with similar DRXed grain sizes and fractions, but distinct c-axes orientations. • In the early extrusion stage, tensile strain along the extrusion direction (ED) promotes basal < a > slip, leading to c-axes rotation toward orientations perpendicular to the ED. • In the later extrusion stage, compressive strain along the normal direction (ND) dominates, activating distinct slip systems under different processing conditions, which results in deviations in the c-axis orientation relative to the ND. AZ31 Mg alloy plates with bimodal grain structures were fabricated via conventional extrusion under varying temperatures and speeds to investigate the mechanisms governing dynamic recrystallization (DRX) and texture evolution. Although all samples exhibited similar DRXed grain sizes (5.0–6.5 µm) and fractions (76%–80%), they developed distinct c-axis orientations and mechanical properties. The P1 sample (350 °C, 0.1 mm/min) exhibited the lowest yield strength (∼192 MPa) but the highest elongation (∼18.2%), whereas the P3 sample (400 °C, 0.6 mm/min) showed the highest yield strength (∼241 MPa) and the lowest elongation (∼14.2%). The P2 sample (400 °C, 0.1 mm/min) demonstrated intermediate behavior (∼226 MPa, ∼17.7%). These variations were primarily attributed to differences in c-axis orientations, particularly their alignment with respect to the normal direction (ND) and their slight deviation from the extrusion direction (ED). Microstructural analysis revealed that distinct DRX mechanisms were activated under different extrusion conditions. P1 predominantly exhibited twinning-induced dynamic recrystallization (TDRX) and continuous dynamic recrystallization (CDRX), whereas P3 primarily showed CDRX and discontinuous dynamic recrystallization (DDRX). These DRX mechanisms, in combination with the activated slip systems governed by the evolving local stress state, collectively contributed to orientation rotation and texture development. During the early stage of extrusion, tensile strain along the ED promoted basal < a > slip, rotating the c-axes toward the ND. As deformation progressed, compressive strain along the ND became dominant. In P1, basal < a > slip remained active, aligning the c-axes along the ND and forming a smaller angle with the ED. In contrast, P3 exhibited predominant pyramidal < c + a > slip, resulting in a pronounced deviation of the c-axes from the ND and a slightly larger angle relative to the ED. The P2 sample exhibited a transitional texture state between those of P1 and P3.

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Publication Details

Journal
Journal of Magnesium and Alloys
Published
2025-09-04
DOI
https://doi.org/10.1016/j.jma.2025.08.004
Citations
3
Primary Topic
Magnesium Alloys: Properties and Applications
Type
article
Field-Weighted Citation Impact
1.79

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article

Unusual texture evolution in extruded AZ31 Mg alloy plates with bimodal grain structures

T. Nakata, Hailong Shi, S. Kamado, Enyu Guo et al.
3 citations
Journal of Magnesium and Alloys
Magnesium Alloys: Properties and Applications
1.79
article

Unusual texture evolution in extruded AZ31 Mg alloy plates with bimodal grain structures

T. Nakata, Hailong Shi, S. Kamado, Enyu Guo, Xuejie Li, Xu Cheng, Zhiyuan Wu, Xiaojun Wang, Hucheng Pan, Lin Geng
article en
3 citations

Abstract

• The microstructural evolution of AZ31 alloy plates during various extrusion processes is analyzed. • The AZ31 Mg alloy plates, extruded via conventional methods under varying temperatures and speeds, exhibit bimodal grain structures with similar DRXed grain sizes and fractions, but distinct c-axes orientations. • In the early extrusion stage, tensile strain along the extrusion direction (ED) promotes basal < a > slip, leading to c-axes rotation toward orientations perpendicular to the ED. • In the later extrusion stage, compressive strain along the normal direction (ND) dominates, activating distinct slip systems under different processing conditions, which results in deviations in the c-axis orientation relative to the ND. AZ31 Mg alloy plates with bimodal grain structures were fabricated via conventional extrusion under varying temperatures and speeds to investigate the mechanisms governing dynamic recrystallization (DRX) and texture evolution. Although all samples exhibited similar DRXed grain sizes (5.0–6.5 µm) and fractions (76%–80%), they developed distinct c-axis orientations and mechanical properties. The P1 sample (350 °C, 0.1 mm/min) exhibited the lowest yield strength (∼192 MPa) but the highest elongation (∼18.2%), whereas the P3 sample (400 °C, 0.6 mm/min) showed the highest yield strength (∼241 MPa) and the lowest elongation (∼14.2%). The P2 sample (400 °C, 0.1 mm/min) demonstrated intermediate behavior (∼226 MPa, ∼17.7%). These variations were primarily attributed to differences in c-axis orientations, particularly their alignment with respect to the normal direction (ND) and their slight deviation from the extrusion direction (ED). Microstructural analysis revealed that distinct DRX mechanisms were activated under different extrusion conditions. P1 predominantly exhibited twinning-induced dynamic recrystallization (TDRX) and continuous dynamic recrystallization (CDRX), whereas P3 primarily showed CDRX and discontinuous dynamic recrystallization (DDRX). These DRX mechanisms, in combination with the activated slip systems governed by the evolving local stress state, collectively contributed to orientation rotation and texture development. During the early stage of extrusion, tensile strain along the ED promoted basal < a > slip, rotating the c-axes toward the ND. As deformation progressed, compressive strain along the ND became dominant. In P1, basal < a > slip remained active, aligning the c-axes along the ND and forming a smaller angle with the ED. In contrast, P3 exhibited predominant pyramidal < c + a > slip, resulting in a pronounced deviation of the c-axes from the ND and a slightly larger angle relative to the ED. The P2 sample exhibited a transitional texture state between those of P1 and P3.

Journal of Magnesium and AlloysVol. 13(10)
Harbin Institute of Technology (CN), Dalian University (CN), Suzhou Research Institute (CN), Nagaoka University of Technology (JP), Northeastern University (CN)
National Natural Science Foundation of China, Harbin Institute of Technology, Natural Science Foundation of Heilongjiang Province, State Key Laboratory of Advanced Welding and Joining, Japan Society for the Promotion of Science, National Key Research and Development Program of China
Openalex Percentile: Top 14%
Magnesium Alloys: Properties and Applications
1.79
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