Ring type furnace integrated into DAC chamber for stable and uniform sample heating up to 2000 K

The diamond anvil cell is a powerful tool for investigating material behavior under extreme pressure and temperature, but achieving efficient and uniform heating remains challenging. This study introduces a ring-type furnace integrated into a gasket with a metal-insulator-metal sandwich structure, using tantalum (Ta) for heating, tungsten (W) for electrodes, and mica-ceramic powder for insulation, enabling stable and uniform heating up to 2000 K. A calibration method combining thermocouple data and finite element simulations ensures accurate temperature measurement. Experimental validation shows that the furnace maintains optical access for spectroscopic measurements and supports in situ conductivity characterization under high-pressure and high-temperature conditions. This advancement provides a robust platform for multi-physics experiments under extreme conditions.

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Publication Details

Journal
Review of Scientific Instruments
Published
2025-09-01
DOI
https://doi.org/10.1063/5.0290862
Primary Topic
High-pressure geophysics and materials
Type
article
Field-Weighted Citation Impact
0.00

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article

Ring type furnace integrated into DAC chamber for stable and uniform sample heating up to 2000 K

Dawei Jiang, Yonghao Han, Min Cao, Wenhui Liu et al.
Review of Scientific Instruments
High-pressure geophysics and materials
article

Ring type furnace integrated into DAC chamber for stable and uniform sample heating up to 2000 K

Dawei Jiang, Yonghao Han, Min Cao, Wenhui Liu, Weichao Li, Muyun Han, Chunxiao Gao
article en

Abstract

The diamond anvil cell is a powerful tool for investigating material behavior under extreme pressure and temperature, but achieving efficient and uniform heating remains challenging. This study introduces a ring-type furnace integrated into a gasket with a metal-insulator-metal sandwich structure, using tantalum (Ta) for heating, tungsten (W) for electrodes, and mica-ceramic powder for insulation, enabling stable and uniform heating up to 2000 K. A calibration method combining thermocouple data and finite element simulations ensures accurate temperature measurement. Experimental validation shows that the furnace maintains optical access for spectroscopic measurements and supports in situ conductivity characterization under high-pressure and high-temperature conditions. This advancement provides a robust platform for multi-physics experiments under extreme conditions.

Review of Scientific InstrumentsVol. 96(9)
Jilin University (CN), Jilin Jianzhu University (CN), Shijiazhuang Tiedao University (CN)
National Key Research and Development Program of China
Openalex Percentile: Top 75%
High-pressure geophysics and materials
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Ring type furnace integrated into DAC chamber for stable and uniform sample heating up to 2000 K — Dawei Jiang, Yonghao Han, et al. · Review of Scientific Instruments (2025) | TGRS Research Map | TGRS