Preparation of a Novel Carbon Nano Coating on Carbon Fiber Surface Based on Plasma Electrolysis Effect

In this study, glucose is used as the source of C; through cathode plasma electrolytic deposition technology, a carbon nano coating is prepared on the surface of carbon fiber. The carbon coating is analyzed using scanning electron microscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy to investigate the effect of pH on the microstructure of the carbon coating on the surface of carbon fiber. At the same time, the oxidation resistance of the coating and the changes in the tensile properties of carbon fiber after high-temperature heat treatment were also investigated. The results showed that reducing the pH value can improve the microstructure of the carbon coating, and the best performance of the carbon coating sample was obtained at pH = 3. The initial oxidation temperature and oxidation termination temperature increased by 156 °C and 110 °C, respectively, compared to the treated carbon fiber but without coating, and the tensile property remains a high value (2740 MPa) after high-temperature heat treatment.