Palladium nanoparticles immobilized in SnFe2O4/SiO2/PM as efficient heterogeneous catalysts for the suzuki cross-coupling reaction

This study focuses on the synthesis of a novel magnetic interphase palladium catalyst immobilized on pyromellitic dianhydride (PM)-coated magnetic SnFe<sub>2</sub>O<sub>4</sub> nanoparticles. Such surface functionalization of magnetic particles represents a promising strategy to bridge the gap between heterogeneous and homogeneous catalysis methods. The structure, morphology, and physicochemical properties of these particles were thoroughly examined using various analytical techniques, including FT-IR, SEM, XRD, VSM, ICP, and EDS. The resulting SnFe<sub>2</sub>O<sub>4</sub>/SiO<sub>2</sub>/PM-Pd nanocatalyst exhibited excellent catalytic performance as a recyclable catalyst in Suzuki-Miyaura cross-coupling reactions at room temperature. Additionally, the catalyst demonstrated high reusability, showing minimal palladium leaching and no significant loss in activity across multiple cycles.

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Publication Details

Journal
Scientific Reports
Published
2025-08-31
DOI
https://doi.org/10.1038/s41598-025-16233-9
Citations
1
Primary Topic
Catalytic Cross-Coupling Reactions
Type
article
Field-Weighted Citation Impact
0.94

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article

Palladium nanoparticles immobilized in SnFe2O4/SiO2/PM as efficient heterogeneous catalysts for the suzuki cross-coupling reaction

Swati Mishra, Jayanti Makasana, Suhas Ballal, Magda H. Abdellattif et al.
1 citations
Scientific Reports
Catalytic Cross-Coupling Reactions
0.94
article

Palladium nanoparticles immobilized in SnFe2O4/SiO2/PM as efficient heterogeneous catalysts for the suzuki cross-coupling reaction

Swati Mishra, Jayanti Makasana, Suhas Ballal, Magda H. Abdellattif, Anjan Kumar, T. Krithiga, Abhayveer Singh, Chou-Yi Hsu, Pushpa Negi Bhakuni, Munther Kadheem
article en
1 citations

Abstract

This study focuses on the synthesis of a novel magnetic interphase palladium catalyst immobilized on pyromellitic dianhydride (PM)-coated magnetic SnFe<sub>2</sub>O<sub>4</sub> nanoparticles. Such surface functionalization of magnetic particles represents a promising strategy to bridge the gap between heterogeneous and homogeneous catalysis methods. The structure, morphology, and physicochemical properties of these particles were thoroughly examined using various analytical techniques, including FT-IR, SEM, XRD, VSM, ICP, and EDS. The resulting SnFe<sub>2</sub>O<sub>4</sub>/SiO<sub>2</sub>/PM-Pd nanocatalyst exhibited excellent catalytic performance as a recyclable catalyst in Suzuki-Miyaura cross-coupling reactions at room temperature. Additionally, the catalyst demonstrated high reusability, showing minimal palladium leaching and no significant loss in activity across multiple cycles.

Scientific ReportsVol. 15(1)
Jain University (IN), Taif University (SA), Siksha O Anusandhan University (IN), Iraqi University (IQ), Marwadi University (IN), Institute of Medical Sciences and Sum Hospital (IN), Sathyabama Institute of Science and Technology (IN), Arizona State University (US), Graphic Era University (IN), Chitkara University (IN), GLA University (IN)
Taif University
Openalex Percentile: Top 22%
Catalytic Cross-Coupling Reactions
0.94
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