Fabrication of Spinel MnCo <sub>2</sub> O <sub>4</sub> Nanocrystal and Its Electrochemical, Magnetic, and Antibacterial Performance

Abstract The spinel MnCo 2 O 4 nanocrystal was effectively synthesized by oil bath co‐precipitation technique. The MnCo 2 O 4 was studied using XRD, FT‐IR, FESEM, and HRTEM techniques to determine its physico‐chemical and surface properties. The FTIR spectrum confirmed the MnCo 2 O 4 nanocrystals' chemical structure, and FESEM and HRTEM analysis revealed their spherical‐like morphologies. The EDS spectrum demonstrated the MnCo 2 O 4 ’s high purity and good crystallinity nature. CV and EIS investigations were used to measure the electrochemical characters of the MnCo 2 O 4 electrode. Using a 2 M tetrabutylammonium perchlorate (TBA) electrolyte, the improved electrode exhibits an extensive potential window of −1.5 to 1.8 V and it delivers the specific capacitance (Cs) of about 673 F/g at 2 mV/s. The MnCo 2 O 4 electrode exhibits specific capacitance values from GCD exhibits 200.4 Fg −1 at 0.5 Ag −1 . The MnCo 2 O 4 electrode achieved capacitive contribution ratios of 72% at s sweep speed of 80 m V s −1 . The magnetic properties of nanoparticles were done by VSM instrument at room temperature. According to the data, MnCo 2 O 4 performed ferromagnetically, with a coercivity field of 28 Oe and a saturation magnetization of 17 emu/g. In addition, we have tested the MnCo 2 O 4 nanospheres for antimicrobial activity against Escherichia coli (E. coli) and Pseudomonas aeruginosa ( P. eruginosa ) and the average zone of inhibition are 10.73 ± 1.18 and 7.33 ± 0.55 mm respectively.

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Journal
ChemistrySelect
Published
2025-08-26
DOI
https://doi.org/10.1002/slct.202503166
Primary Topic
Transition Metal Oxide Nanomaterials
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article
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article

Fabrication of Spinel MnCo 2 O 4 Nanocrystal and Its Electrochemical, Magnetic, and Antibacterial Performance

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Fabrication of Spinel MnCo 2 O 4 Nanocrystal and Its Electrochemical, Magnetic, and Antibacterial Performance

G. Srinivasan, G. Pradeesh, M. Shanthi Thangam, R. Boopathiraja, K. Vishwanathan, P. Suresh, L. Guganathan, M. Silambarasan, S. Ramu, H. Pooja Shakshi
article en

Abstract

Abstract The spinel MnCo 2 O 4 nanocrystal was effectively synthesized by oil bath co‐precipitation technique. The MnCo 2 O 4 was studied using XRD, FT‐IR, FESEM, and HRTEM techniques to determine its physico‐chemical and surface properties. The FTIR spectrum confirmed the MnCo 2 O 4 nanocrystals' chemical structure, and FESEM and HRTEM analysis revealed their spherical‐like morphologies. The EDS spectrum demonstrated the MnCo 2 O 4 ’s high purity and good crystallinity nature. CV and EIS investigations were used to measure the electrochemical characters of the MnCo 2 O 4 electrode. Using a 2 M tetrabutylammonium perchlorate (TBA) electrolyte, the improved electrode exhibits an extensive potential window of −1.5 to 1.8 V and it delivers the specific capacitance (Cs) of about 673 F/g at 2 mV/s. The MnCo 2 O 4 electrode exhibits specific capacitance values from GCD exhibits 200.4 Fg −1 at 0.5 Ag −1 . The MnCo 2 O 4 electrode achieved capacitive contribution ratios of 72% at s sweep speed of 80 m V s −1 . The magnetic properties of nanoparticles were done by VSM instrument at room temperature. According to the data, MnCo 2 O 4 performed ferromagnetically, with a coercivity field of 28 Oe and a saturation magnetization of 17 emu/g. In addition, we have tested the MnCo 2 O 4 nanospheres for antimicrobial activity against Escherichia coli (E. coli) and Pseudomonas aeruginosa ( P. eruginosa ) and the average zone of inhibition are 10.73 ± 1.18 and 7.33 ± 0.55 mm respectively.

ChemistrySelectVol. 10(33)
Department of Biotechnology (IN), Swami Vivekanand College of Pharmacy (IN), Rajabhat Maha Sarakham University (TH), Sathyabama Institute of Science and Technology (IN), Saveetha University (IN)
Openalex Percentile: Top 81%
Transition Metal Oxide Nanomaterials
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