Microstructure, mechanical properties, and fatigue performance of a PBF-LB Al2139ZrTi alloy

• PBF-LB Al2139ZrTi forms fine (∼1.5 µm), equiaxed grains with stable dispersoid phases. • Post-aging yields 573 MPa UTS and 6.5 % elongation via multiscale strengthening. • Fatigue cracks start at surface defects; VHCF cracks show fisheyes at depth. • Endurance limit ∼ 116 MPa; consistent across conventional and VHCF regimes. • Defect control is key for HCF and VHCF design with PBF-LB Al2139ZrTi. This study investigates the microstructure, tensile, and fatigue behavior of post-aged powder bed fused-laser beam (PBF-LB) Al2139ZrTi alloy, developed by EOS North America. The microstructure exhibits an equiaxed grain structure with an average grain size of approximately 1.5 µm and lacks any strong crystallographic texture. It also contains a dense dispersion of fine, uniformly distributed precipitates including: (i) Al 3 (Zr,Ti) dispersoids with L1 2 -type structure, acting as semi-coherent nucleation sites that contribute to grain refinement; (ii) a unique Al 3 (Zr,Ti) plate-like phase, further confirming Zr–Ti-driven modification of precipitation pathways; (iii) Al(CuFeMn) and Al(MnCu) intermetallics, notably Al 7 Cu 2 (Fe,Mn) and Al 20 Cu 2 Mn 3 (T-phase), and (iv) Mg oxides, pointing to minor oxidation during processing. Notably, Al 2 Cu-based θ′ and Ω phases are sparse, with only coarse θ-phase particles (∼0.5–1 µm) at grain boundaries and fine plate-like Ω-phase (∼tens of nm thick) along the [100] zone axis. Mechanical properties were evaluated via tensile testing, yielding ∼ 470 MPa yield stress (YS), ∼570 MPa ultimate tensile strength (UTS), and ∼ 6.5 % elongation. Conventional (servo-hydraulic) and ultrasonic fatigue tests were performed to cover high cycle and very high cycle fatigue responses spanning up to 10 9 cycles. Fractographic analyses, including optical and electron microscopy techniques, were carried out to quantify the crack initiation mechanisms in the mentioned regimes.

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Publication Details

Journal
International Journal of Fatigue
Published
2025-08-20
DOI
https://doi.org/10.1016/j.ijfatigue.2025.109245
Primary Topic
Aluminum Alloys Composites Properties
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article
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article

Microstructure, mechanical properties, and fatigue performance of a PBF-LB Al2139ZrTi alloy

Marta Gajewska, Shawkat Imam Shakil, Meysam Haghshenas, Zaynab Mahbooba et al.
International Journal of Fatigue
Aluminum Alloys Composites Properties
article

Microstructure, mechanical properties, and fatigue performance of a PBF-LB Al2139ZrTi alloy

Marta Gajewska, Shawkat Imam Shakil, Meysam Haghshenas, Zaynab Mahbooba, Andrea Tridello, Wiktor Bednarczyk, Ankit Saharan, Alessandro Benelli
article en

Abstract

• PBF-LB Al2139ZrTi forms fine (∼1.5 µm), equiaxed grains with stable dispersoid phases. • Post-aging yields 573 MPa UTS and 6.5 % elongation via multiscale strengthening. • Fatigue cracks start at surface defects; VHCF cracks show fisheyes at depth. • Endurance limit ∼ 116 MPa; consistent across conventional and VHCF regimes. • Defect control is key for HCF and VHCF design with PBF-LB Al2139ZrTi. This study investigates the microstructure, tensile, and fatigue behavior of post-aged powder bed fused-laser beam (PBF-LB) Al2139ZrTi alloy, developed by EOS North America. The microstructure exhibits an equiaxed grain structure with an average grain size of approximately 1.5 µm and lacks any strong crystallographic texture. It also contains a dense dispersion of fine, uniformly distributed precipitates including: (i) Al 3 (Zr,Ti) dispersoids with L1 2 -type structure, acting as semi-coherent nucleation sites that contribute to grain refinement; (ii) a unique Al 3 (Zr,Ti) plate-like phase, further confirming Zr–Ti-driven modification of precipitation pathways; (iii) Al(CuFeMn) and Al(MnCu) intermetallics, notably Al 7 Cu 2 (Fe,Mn) and Al 20 Cu 2 Mn 3 (T-phase), and (iv) Mg oxides, pointing to minor oxidation during processing. Notably, Al 2 Cu-based θ′ and Ω phases are sparse, with only coarse θ-phase particles (∼0.5–1 µm) at grain boundaries and fine plate-like Ω-phase (∼tens of nm thick) along the [100] zone axis. Mechanical properties were evaluated via tensile testing, yielding ∼ 470 MPa yield stress (YS), ∼570 MPa ultimate tensile strength (UTS), and ∼ 6.5 % elongation. Conventional (servo-hydraulic) and ultrasonic fatigue tests were performed to cover high cycle and very high cycle fatigue responses spanning up to 10 9 cycles. Fractographic analyses, including optical and electron microscopy techniques, were carried out to quantify the crack initiation mechanisms in the mentioned regimes.

International Journal of FatigueVol. 202
Jagiellonian University (PL), Politecnico di Torino (IT), Pflugerville Independent School District (US), AGH University of Krakow (PL), University of Toledo (US)
Affordable and clean energy
Openalex Percentile: Top 79%
Aluminum Alloys Composites Properties
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