Preparation of Arylidene Sulfacetamide Reduced Graphene Oxide Nanocomposites and Measure some of its Optical Properties

Nanocomposites based on Schiff base reactions with reduced graphene oxide were prepared, and their optical and mechanical properties were studied. The preparation methods included synthesizing Schiff bases using sulfacetamide and aromatic benzaldehydes, preparing graphene oxide via the modified Hummer's method, and reducing it with aqueous hydrazine. Infrared spectroscopy (FTIR) and (NMR) analyses confirmed the successful formation of the nanocomposites. The results revealed that the prepared composites exhibit unique properties, with optical transmittance increasing variably between 49% and 89%, and energy band gaps ranging from 3.5 to 4.0 eV. Scanning Electron Microscope (SEM) images demonstrated that these composites possess distinctive nanostructures, enhancing their hydrogen bonding capability and increasing their effective surface area. These properties make the composites suitable for diverse applications in optical, magnetic, and mechanical fields.

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Publication Details

Journal
International Journal of Sustainable Applied Sciences
Published
2025-06-24
DOI
https://doi.org/10.59890/ijsas.v3i6.53
Primary Topic
Conducting polymers and applications
Type
article
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article

Preparation of Arylidene Sulfacetamide Reduced Graphene Oxide Nanocomposites and Measure some of its Optical Properties

Ghazwan H. Al-Somaidaie, Tareq Bandar Mahmood, Yousuf Mohammed, Awais Ahmad
International Journal of Sustainable Applied Sciences
Conducting polymers and applications
article

Preparation of Arylidene Sulfacetamide Reduced Graphene Oxide Nanocomposites and Measure some of its Optical Properties

Ghazwan H. Al-Somaidaie, Tareq Bandar Mahmood, Yousuf Mohammed, Awais Ahmad
article en

Abstract

Nanocomposites based on Schiff base reactions with reduced graphene oxide were prepared, and their optical and mechanical properties were studied. The preparation methods included synthesizing Schiff bases using sulfacetamide and aromatic benzaldehydes, preparing graphene oxide via the modified Hummer's method, and reducing it with aqueous hydrazine. Infrared spectroscopy (FTIR) and (NMR) analyses confirmed the successful formation of the nanocomposites. The results revealed that the prepared composites exhibit unique properties, with optical transmittance increasing variably between 49% and 89%, and energy band gaps ranging from 3.5 to 4.0 eV. Scanning Electron Microscope (SEM) images demonstrated that these composites possess distinctive nanostructures, enhancing their hydrogen bonding capability and increasing their effective surface area. These properties make the composites suitable for diverse applications in optical, magnetic, and mechanical fields.

International Journal of Sustainable Applied SciencesVol. 3(6)
University of Baghdad (IQ), University of Anbar (IQ), Salesian University (MX), University of Tikrit (IQ)
Affordable and clean energy
Openalex Percentile: Top 83%
Conducting polymers and applications
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