Impact of sodium on acetone sensing behaviour of ZnO prepared by microwave-assisted combustion method

Herein, we have reported the preparation, characterization, and acetone sensing properties of ZnO, 2%,5%, and 10% Na-doped ZnO samples synthesized using the microwave-assisted combustion method, aimed to enhance the sensitivity at low temperatures. The prepared samples were characterized using several characterization techniques to analyze their phase structure, crystallinity, and morphology. X-ray diffraction (XRD) analysis confirmed that the synthesized ZnO samples possess a well-crystalline hexagonal wurtzite crystal structure. The detailed experiments revealed that at an optimized temperature, i.e., ~ 50 °C, 5% Na-ZnO sample exhibited a significant sensitivity towards acetone concentrations of 100, 200, 300, 400, and 500 ppm with response value of ~ 39, ~54, ~ 100, ~214, and ~ 300% and the response and recovery time of ~ 442 /~62 s, respectively. The results indicate that 5% Na-ZnO samples have a high sensing response towards acetone at low operating temperatures.

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Publication Details

Journal
Discover Materials
Published
2025-07-24
DOI
https://doi.org/10.1007/s43939-025-00340-5
Primary Topic
Gas Sensing Nanomaterials and Sensors
Type
article
Field-Weighted Citation Impact
0.00

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article

Impact of sodium on acetone sensing behaviour of ZnO prepared by microwave-assisted combustion method

Sumit Mishra, Anurag Shukla, Brajendra Singh, Divyanshu Singh
Discover Materials
Gas Sensing Nanomaterials and Sensors
article

Impact of sodium on acetone sensing behaviour of ZnO prepared by microwave-assisted combustion method

Sumit Mishra, Anurag Shukla, Brajendra Singh, Divyanshu Singh
article en

Abstract

Herein, we have reported the preparation, characterization, and acetone sensing properties of ZnO, 2%,5%, and 10% Na-doped ZnO samples synthesized using the microwave-assisted combustion method, aimed to enhance the sensitivity at low temperatures. The prepared samples were characterized using several characterization techniques to analyze their phase structure, crystallinity, and morphology. X-ray diffraction (XRD) analysis confirmed that the synthesized ZnO samples possess a well-crystalline hexagonal wurtzite crystal structure. The detailed experiments revealed that at an optimized temperature, i.e., ~ 50 °C, 5% Na-ZnO sample exhibited a significant sensitivity towards acetone concentrations of 100, 200, 300, 400, and 500 ppm with response value of ~ 39, ~54, ~ 100, ~214, and ~ 300% and the response and recovery time of ~ 442 /~62 s, respectively. The results indicate that 5% Na-ZnO samples have a high sensing response towards acetone at low operating temperatures.

Discover MaterialsVol. 5(1)
University of Allahabad (IN)
Department of Science and Technology, Ministry of Science and Technology, India
Affordable and clean energy
Openalex Percentile: Top 83%
Gas Sensing Nanomaterials and Sensors
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