A Modified Two-Temperature Calibration Method and Facility for Emissivity Measurement

Measuring the emissivity of an infrared radiant sample with high accuracy is important. Previous studies reported on the multi- or two-temperature calibration methods, which used a reference blackbody (or blackbodies) to eliminate the background radiation, and assumed that the background radiation was independent of temperature. However, in practical measurements, this assumption does not hold. To solve the above problems, this study proposes a modified two-temperature calibration method and facility. The two temperature points are set in a certain small interval based on the proposed calculation method; based on the indication of the approximation that the emissivities of the sample and the background radiations remain the same at these two temperatures, the emissivities can be calculated with measurement signals at these two temperatures, and a reference blackbody is not needed. An experimental facility was built up and three samples with emissivities around 0.100, 0.500, and 0.900 were measured in (8~14) μm. The relative expanded uncertainties were 9.6%, 4.0%, and 1.5% at 60 °C, respectively, and 8.8%, 5.8%, and 1.2% at 85 °C (<i>k</i> = 2), respectively. The experimental results showed consistency with the results obtained using other methods, indicating the effectiveness of the developed method. The developed method might be suitable for samples whose emissivities are temperature insensitive.

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Publication Details

Journal
Materials
Published
2025-07-19
DOI
https://doi.org/10.3390/ma18143392
Citations
1
Primary Topic
Calibration and Measurement Techniques
Type
article
Field-Weighted Citation Impact
4.99

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A Modified Two-Temperature Calibration Method and Facility for Emissivity Measurement

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A Modified Two-Temperature Calibration Method and Facility for Emissivity Measurement

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article en
1 citations

Abstract

Measuring the emissivity of an infrared radiant sample with high accuracy is important. Previous studies reported on the multi- or two-temperature calibration methods, which used a reference blackbody (or blackbodies) to eliminate the background radiation, and assumed that the background radiation was independent of temperature. However, in practical measurements, this assumption does not hold. To solve the above problems, this study proposes a modified two-temperature calibration method and facility. The two temperature points are set in a certain small interval based on the proposed calculation method; based on the indication of the approximation that the emissivities of the sample and the background radiations remain the same at these two temperatures, the emissivities can be calculated with measurement signals at these two temperatures, and a reference blackbody is not needed. An experimental facility was built up and three samples with emissivities around 0.100, 0.500, and 0.900 were measured in (8~14) μm. The relative expanded uncertainties were 9.6%, 4.0%, and 1.5% at 60 °C, respectively, and 8.8%, 5.8%, and 1.2% at 85 °C (<i>k</i> = 2), respectively. The experimental results showed consistency with the results obtained using other methods, indicating the effectiveness of the developed method. The developed method might be suitable for samples whose emissivities are temperature insensitive.

MaterialsVol. 18(14)
Beijing Institute of Petrochemical Technology (CN), National Institute of Metrology (CN)
National Natural Science Foundation of China, China Postdoctoral Science Foundation, National Institute of Metrology, China
Affordable and clean energy
Openalex Percentile: Top 5%
Calibration and Measurement Techniques
4.99
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