Hot isostatic pressing elimination of process-induced defects in laser powder bed fusion fabricated DZ125 superalloy: Microstructure evolution and mechanical property enhancement

This study systematically investigated the crack formation mechanisms in DZ125 nickel-based superalloy fabricated by laser powder bed fusion (LPBF) and evaluated the effectiveness of hot isostatic pressing (HIP) in defect elimination, microstructural modification, and mechanical property enhancement. The results revealed that the cracks in LPBF-processed DZ125 alloy are primarily solidification cracks and liquation cracks, whose formation is associated with thermal stress concentration and low-melting-point eutectic phases induced by segregation of Hf/Ti elements. The conduction-mode melt pools (with an aspect ratio ≈0.5) formed at high scanning speeds effectively mitigated crack formation. After HIP treatments at different temperatures (1050°C, 1150°C, and 1230°C), both cracks and pores were significantly reduced, with near-complete densification and almost full recrystallization achieved at 1230°C. Increasing HIP temperature leads to γ′ phase coarsening and columnar-to-equiaxed grain transformation. The 1050°C-HIP samples exhibited enhanced yield strength (859 MPa) due to precipitation of fine γ′ phases (∼100 nm), while the 1150°C and 1230°C-HIP samples show reduced yield strength but significantly improved elongation (17.5% and 21.8%, respectively) owing to γ′ coarsening and recrystallization. This work provides crucial insights for defect control and performance optimization of LPBF-fabricated DZ125 superalloy.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-07-01
DOI
https://doi.org/10.1016/j.jmrt.2025.07.069
Citations
7
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
4.99

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article

Hot isostatic pressing elimination of process-induced defects in laser powder bed fusion fabricated DZ125 superalloy: Microstructure evolution and mechanical property enhancement

Jikang Li, Qingsong Wei, Jiangtao Sun, Boyu Wu et al.
7 citations
Journal of Materials Research and Technology
Additive Manufacturing Materials and Processes
4.99
article

Hot isostatic pressing elimination of process-induced defects in laser powder bed fusion fabricated DZ125 superalloy: Microstructure evolution and mechanical property enhancement

Jikang Li, Qingsong Wei, Jiangtao Sun, Boyu Wu, Wei Li, Chao Cai, Honghao Xiang, Zhenwu Zhang, Hairui Gao
article en
7 citations

Abstract

This study systematically investigated the crack formation mechanisms in DZ125 nickel-based superalloy fabricated by laser powder bed fusion (LPBF) and evaluated the effectiveness of hot isostatic pressing (HIP) in defect elimination, microstructural modification, and mechanical property enhancement. The results revealed that the cracks in LPBF-processed DZ125 alloy are primarily solidification cracks and liquation cracks, whose formation is associated with thermal stress concentration and low-melting-point eutectic phases induced by segregation of Hf/Ti elements. The conduction-mode melt pools (with an aspect ratio ≈0.5) formed at high scanning speeds effectively mitigated crack formation. After HIP treatments at different temperatures (1050°C, 1150°C, and 1230°C), both cracks and pores were significantly reduced, with near-complete densification and almost full recrystallization achieved at 1230°C. Increasing HIP temperature leads to γ′ phase coarsening and columnar-to-equiaxed grain transformation. The 1050°C-HIP samples exhibited enhanced yield strength (859 MPa) due to precipitation of fine γ′ phases (∼100 nm), while the 1150°C and 1230°C-HIP samples show reduced yield strength but significantly improved elongation (17.5% and 21.8%, respectively) owing to γ′ coarsening and recrystallization. This work provides crucial insights for defect control and performance optimization of LPBF-fabricated DZ125 superalloy.

Journal of Materials Research and TechnologyVol. 37
Beijing Research Institute of Mechanical and Electrical Technology (CN), Wuhan University of Science and Technology (CN), Huazhong University of Science and Technology (CN)
National Natural Science Foundation of China, Hebei Provincial Key Research Projects
Openalex Percentile: Top 4%
Additive Manufacturing Materials and Processes
4.99
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