Influence of vanadium carbides and stacking fault energy on the low-cycle fatigue behavior of a face-centered cubic multi-principal element alloy

• The addition of 2.5 wt.-% V and 1.5-wt.% C to the Fe-30Mn-10Co-10Cr MPEA led to the pronounced formation of nm-sized VC precipitates in an fcc matrix. • Strain-controlled fatigue tests between Δε/2 = 0.2 - 0.8 % revealed an increase in LCF and HCF performance between 40.8 and 62.1 % • Precipitation of VC led to a change from TWIP- to TRIP-dominated deformation behavior due to decreased C-content in the matrix, which resulted in decreased SFE. • The reduction of the SFE led to increased slip planarity and reversibility, further improving fatigue resistance. Multi-principal element alloys (MPEA) have gathered significant attention in the scientific community due to their versatility and design concepts. The Fe30Mn10Co10Cr (at.-%) MPEA system revealed outstanding mechanical properties, owing to the activation of multiple strengthening mechanisms. In this MPEA system, the formation of vanadium carbides was found to be efficient to enhance the strength and to provide further design flexibility. However, the low-cycle fatigue behavior has not yet been investigated. To address this, a fully recrystallized, single-phase face-centered cubic (fcc) structure and a recrystallized and aged state that was strengthened by a uniform distribution of 6.5 % nanosized vanadium carbides were evaluated. It was revealed that the aged samples exhibited a notable improvement in cyclic fatigue performance. The precipitation of vanadium carbides led to a reduction in solute carbon content in the fcc matrix, which in turn resulted in the transformation-induced plasticity effect becoming the dominant deformation mechanism in the aged samples. This was coupled with a decrease in plastic strain amplitude and an increase in slip reversibility. As a result, the number of cycles to failure in the low-cycle fatigue regime increased by 40.8 % to 62.1 %, facilitating the concurrent optimization of both tensile and fatigue properties.

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Publication Details

Journal
International Journal of Fatigue
Published
2025-07-05
DOI
https://doi.org/10.1016/j.ijfatigue.2025.109158
Citations
1
Primary Topic
High Entropy Alloys Studies
Type
article
Field-Weighted Citation Impact
0.71
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article

Influence of vanadium carbides and stacking fault energy on the low-cycle fatigue behavior of a face-centered cubic multi-principal element alloy

Hans Jürgen Maier, Ulrich Krupp, Steffen Wackenrohr, Christian Hinte et al.
1 citations
International Journal of Fatigue
High Entropy Alloys Studies
0.71
article

Influence of vanadium carbides and stacking fault energy on the low-cycle fatigue behavior of a face-centered cubic multi-principal element alloy

Hans Jürgen Maier, Ulrich Krupp, Steffen Wackenrohr, Christian Hinte, Felix Oppermann, Christian Haase
article en
1 citations

Abstract

• The addition of 2.5 wt.-% V and 1.5-wt.% C to the Fe-30Mn-10Co-10Cr MPEA led to the pronounced formation of nm-sized VC precipitates in an fcc matrix. • Strain-controlled fatigue tests between Δε/2 = 0.2 - 0.8 % revealed an increase in LCF and HCF performance between 40.8 and 62.1 % • Precipitation of VC led to a change from TWIP- to TRIP-dominated deformation behavior due to decreased C-content in the matrix, which resulted in decreased SFE. • The reduction of the SFE led to increased slip planarity and reversibility, further improving fatigue resistance. Multi-principal element alloys (MPEA) have gathered significant attention in the scientific community due to their versatility and design concepts. The Fe30Mn10Co10Cr (at.-%) MPEA system revealed outstanding mechanical properties, owing to the activation of multiple strengthening mechanisms. In this MPEA system, the formation of vanadium carbides was found to be efficient to enhance the strength and to provide further design flexibility. However, the low-cycle fatigue behavior has not yet been investigated. To address this, a fully recrystallized, single-phase face-centered cubic (fcc) structure and a recrystallized and aged state that was strengthened by a uniform distribution of 6.5 % nanosized vanadium carbides were evaluated. It was revealed that the aged samples exhibited a notable improvement in cyclic fatigue performance. The precipitation of vanadium carbides led to a reduction in solute carbon content in the fcc matrix, which in turn resulted in the transformation-induced plasticity effect becoming the dominant deformation mechanism in the aged samples. This was coupled with a decrease in plastic strain amplitude and an increase in slip reversibility. As a result, the number of cycles to failure in the low-cycle fatigue regime increased by 40.8 % to 62.1 %, facilitating the concurrent optimization of both tensile and fatigue properties.

International Journal of FatigueVol. 201
Leibniz University Hannover (DE), Technische Universität Berlin (DE), RWTH Aachen University (DE)
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Openalex Percentile: Top 30%
High Entropy Alloys Studies
0.71
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