Synthesis of 6-methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation

Apparently, many students spend a lot of time doing column chromatography, and in many cases they describe the process as "difficult", "time-consuming", or "tedious".Often, they would collect numerous fractions, use large amount of solvents even for scales ~100 mg, and routinely spend more than 1 hr or multiple hours just on one column.

Authors

Publication Details

Journal
Organic Syntheses
Published
2025-01-01
DOI
https://doi.org/10.15227/orgsyn.102.0335
Citations
1
Primary Topic
Synthesis of Organic Compounds
Type
article
Field-Weighted Citation Impact
1.39
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article

Synthesis of 6-methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation

Stephen A. Chamness
1 citations
Organic Syntheses
Synthesis of Organic Compounds
1.39
article

Synthesis of 6-methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation

Stephen A. Chamness
article en
1 citations

Abstract

Apparently, many students spend a lot of time doing column chromatography, and in many cases they describe the process as "difficult", "time-consuming", or "tedious".Often, they would collect numerous fractions, use large amount of solvents even for scales ~100 mg, and routinely spend more than 1 hr or multiple hours just on one column.

Organic SynthesesVol. 102
Openalex Percentile: Top 19%
Synthesis of Organic Compounds
1.39
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Synthesis of 6-methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation — Stephen A. Chamness · Organic Syntheses (2025) | TGRS Research Map | TGRS