MDT: A simple tool to facilitate dropcasting on in situ TEM MEMS chips

<i>In situ</i> transmission electron microscopy with holders based on the use of micro-electromechanical systems provides valuable insights into material kinetics, yet sample preparation remains complex due to fragile silicon nitride (Si<sub>3</sub>N<sub>4</sub>) windows and the risk of leaks and contamination during dropcasting. This results in failed experiments and increases experimental costs. This paper introduces the MEMS Dropcasting Tool (MDT), a cost-effective, in-house 3D-printable solution that confines the droplet to a specific area, preventing particle migration under the O-ring and reducing contamination risks at the inlet and outlet ports of closed cell chip holders.

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Publication Details

Journal
HardwareX
Published
2025-06-21
DOI
https://doi.org/10.1016/j.ohx.2025.e00666
Primary Topic
Nanowire Synthesis and Applications
Type
article
Field-Weighted Citation Impact
0.00

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article

MDT: A simple tool to facilitate dropcasting on in situ TEM MEMS chips

Joke Hadermann, Matthias Quintelier
HardwareX
Nanowire Synthesis and Applications
article

MDT: A simple tool to facilitate dropcasting on in situ TEM MEMS chips

Joke Hadermann, Matthias Quintelier
article en

Abstract

<i>In situ</i> transmission electron microscopy with holders based on the use of micro-electromechanical systems provides valuable insights into material kinetics, yet sample preparation remains complex due to fragile silicon nitride (Si<sub>3</sub>N<sub>4</sub>) windows and the risk of leaks and contamination during dropcasting. This results in failed experiments and increases experimental costs. This paper introduces the MEMS Dropcasting Tool (MDT), a cost-effective, in-house 3D-printable solution that confines the droplet to a specific area, preventing particle migration under the O-ring and reducing contamination risks at the inlet and outlet ports of closed cell chip holders.

HardwareXVol. 23
University of Antwerp (BE)
Universiteit Antwerpen
Openalex Percentile: Top 87%
Nanowire Synthesis and Applications
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