Microstructure and texture evolution of the oxide scale on hot rolled corrosion-resistant steel

The texture evolution and microstructure transformation of scale on high-strength, corrosion-resistant steel during hot rolling were studied through simulated rolling in a laboratory and electron backscattering diffraction analysis in a scanning electron microscope. The results showed that the Fe 3 O 4 phase in the scale had dual-phase isomerism, with the Fe 3 O 4 phase in the oxide layer and at the interface of the oxide layer and matrix having columnar crystal and equiaxed spherical morphologies, respectively. The FeO phase forms a strong fiber texture in the{100}direction, and the triangular Fe 2 O 3 phase forms a fiber texture in the{0001}direction. As the reduction rate increases from 12% to 20%, the{110}< > texture of Fe 3 O 4 changes to{112}< >, and the Schmidt factor decreases from 0.4841 to 0.4232. The grains with a higher Schmidt factor could undergo plastic deformation earlier than those with a lower Schmidt factor. The introduction of the Schmidt factor clarified the behavior of texture evolution during high-temperature plastic deformation. The formation of fine-grained Fe 3 O 4 at the interface of steel matrix is governed by the stress relief mechanism.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-06-18
DOI
https://doi.org/10.1016/j.jmrt.2025.06.129
Citations
2
Primary Topic
High-Temperature Coating Behaviors
Type
article
Field-Weighted Citation Impact
9.99
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article

Microstructure and texture evolution of the oxide scale on hot rolled corrosion-resistant steel

Huibin Wu, Youyou Zhang, Chao Wang
2 citations
Journal of Materials Research and Technology
High-Temperature Coating Behaviors
9.99
article

Microstructure and texture evolution of the oxide scale on hot rolled corrosion-resistant steel

Huibin Wu, Youyou Zhang, Chao Wang
article en
2 citations

Abstract

The texture evolution and microstructure transformation of scale on high-strength, corrosion-resistant steel during hot rolling were studied through simulated rolling in a laboratory and electron backscattering diffraction analysis in a scanning electron microscope. The results showed that the Fe 3 O 4 phase in the scale had dual-phase isomerism, with the Fe 3 O 4 phase in the oxide layer and at the interface of the oxide layer and matrix having columnar crystal and equiaxed spherical morphologies, respectively. The FeO phase forms a strong fiber texture in the{100}direction, and the triangular Fe 2 O 3 phase forms a fiber texture in the{0001}direction. As the reduction rate increases from 12% to 20%, the{110}< > texture of Fe 3 O 4 changes to{112}< >, and the Schmidt factor decreases from 0.4841 to 0.4232. The grains with a higher Schmidt factor could undergo plastic deformation earlier than those with a lower Schmidt factor. The introduction of the Schmidt factor clarified the behavior of texture evolution during high-temperature plastic deformation. The formation of fine-grained Fe 3 O 4 at the interface of steel matrix is governed by the stress relief mechanism.

Journal of Materials Research and TechnologyVol. 37
University of Science and Technology Liaoning (CN), Liaoning University (CN), University of Science and Technology Beijing (CN), Tsinghua University (CN)
Openalex Percentile: Top 3%
High-Temperature Coating Behaviors
9.99
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