Influence of Incubation Duration on Bond Strength and Microhardness of Calcium Silicate‐Based Materials

The objective of this study was to investigate the effect of different incubation periods on the push-out bond strength and microhardness of calcium-silicate-based materials: MTA-Angelus, Biodentine and BIOfactor MTA. A total of 100 dentine discs were used for the push-out test. Three cavities were prepared on each dentine disc. Each cavity on the same disc was filled with MTA-Angelus, Biodentine or BIOfactor MTA. Half of the dentine samples were incubated at 37°C for 1 day, and the other half for 28 days (n = 50). Push-out testing was then performed. For the microhardness test, material discs were prepared by mixing the materials and placing them into Teflon moulds (n = 26). The samples were incubated at 37°C for either 1 day or 28 days (n = 13). Vickers microhardness testing was conducted. The data were statistically analysed. The results showed that Biodentine exhibited the highest bond strength and microhardness at both time points, while MTA-Angelus showed the lowest (p < 0.05). Overall, Biodentine demonstrated superior performance, while BIOfactor MTA showed promising but moderate results.

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Publication Details

Journal
Australian Endodontic Journal
Published
2025-06-06
DOI
https://doi.org/10.1111/aej.12961
Primary Topic
Endodontics and Root Canal Treatments
Type
article
Field-Weighted Citation Impact
0.00

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article

Influence of Incubation Duration on Bond Strength and Microhardness of Calcium Silicate‐Based Materials

Makbule Bilge Akbulut, Emine Şimşek
Australian Endodontic Journal
Endodontics and Root Canal Treatments
article

Influence of Incubation Duration on Bond Strength and Microhardness of Calcium Silicate‐Based Materials

Makbule Bilge Akbulut, Emine Şimşek
article en

Abstract

The objective of this study was to investigate the effect of different incubation periods on the push-out bond strength and microhardness of calcium-silicate-based materials: MTA-Angelus, Biodentine and BIOfactor MTA. A total of 100 dentine discs were used for the push-out test. Three cavities were prepared on each dentine disc. Each cavity on the same disc was filled with MTA-Angelus, Biodentine or BIOfactor MTA. Half of the dentine samples were incubated at 37°C for 1 day, and the other half for 28 days (n = 50). Push-out testing was then performed. For the microhardness test, material discs were prepared by mixing the materials and placing them into Teflon moulds (n = 26). The samples were incubated at 37°C for either 1 day or 28 days (n = 13). Vickers microhardness testing was conducted. The data were statistically analysed. The results showed that Biodentine exhibited the highest bond strength and microhardness at both time points, while MTA-Angelus showed the lowest (p < 0.05). Overall, Biodentine demonstrated superior performance, while BIOfactor MTA showed promising but moderate results.

Australian Endodontic JournalVol. 51(2)
Necmettin Erbakan University (TR), Mersin Üniversitesi (TR)
Necmettin Erbakan Üniversitesi
Openalex Percentile: Top 82%
Endodontics and Root Canal Treatments
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