Compact laser-induced plasma source for advanced soft X-ray absorption spectroscopy

X-ray absorption spectroscopy is a key method for compositional analysis, probing electronic transitions from core to unoccupied states. Traditionally, this technique requires large-scale facilities like synchrotrons due to the high photon flux needed, especially in the soft X-ray range. Recent developments in table-top soft X-ray sources now offer a laboratory-scale alternative. We present our compact, pulsed gas-target laser-induced plasma source using a krypton jet, producing debris-free radiation from 250 to 1000 eV. Integrated with a high line-density flat-field grating, our spectrometer achieves a resolution of up to E/ΔE = 1535 at 430 eV, allowing multi-edge analysis. This system effectively resolves K- and L-edges of various elements and supports both solid and liquid thin samples. Using a thin lamella in vacuum for liquid samples expands analysis capabilities. Excellent synchrotron comparison highlights this system’s potential as an accessible alternative for routine, high-precision measurements.

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Published
2025-06-06
DOI
https://doi.org/10.1117/12.3056486
Primary Topic
X-ray Spectroscopy and Fluorescence Analysis
Type
article
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article

Compact laser-induced plasma source for advanced soft X-ray absorption spectroscopy

Bernd Abel, G. Marowsky, Jonathan Holburg, L. Sölter et al.
X-ray Spectroscopy and Fluorescence Analysis
article

Compact laser-induced plasma source for advanced soft X-ray absorption spectroscopy

Bernd Abel, G. Marowsky, Jonathan Holburg, L. Sölter, Anja Ahrens, Aleš Charvát, Maik Lübbecke, Dong‐Du Mai, Stephan Figul, Klaus Mann, Jürgen Thieme
article en

Abstract

X-ray absorption spectroscopy is a key method for compositional analysis, probing electronic transitions from core to unoccupied states. Traditionally, this technique requires large-scale facilities like synchrotrons due to the high photon flux needed, especially in the soft X-ray range. Recent developments in table-top soft X-ray sources now offer a laboratory-scale alternative. We present our compact, pulsed gas-target laser-induced plasma source using a krypton jet, producing debris-free radiation from 250 to 1000 eV. Integrated with a high line-density flat-field grating, our spectrometer achieves a resolution of up to E/ΔE = 1535 at 430 eV, allowing multi-edge analysis. This system effectively resolves K- and L-edges of various elements and supports both solid and liquid thin samples. Using a thin lamella in vacuum for liquid samples expands analysis capabilities. Excellent synchrotron comparison highlights this system’s potential as an accessible alternative for routine, high-precision measurements.

Institut für Nanophotonik (DE), Institut für Nichtklassische Chemie (DE), University of Göttingen (DE), Leipzig University (DE)
Affordable and clean energy
Openalex Percentile: Top 81%
X-ray Spectroscopy and Fluorescence Analysis
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Compact laser-induced plasma source for advanced soft X-ray absorption spectroscopy — Bernd Abel, G. Marowsky, et al. · (2025) | TGRS Research Map | TGRS