A new compact setup for in-situ grazing incidence X-ray experiments of solid and liquid samples

Abstract A compact new X-ray reflectometer setup was realized, with a main design focus on mechanical stability and ruggedness, allowing in particular the change from a horizontal to a vertical scattering geometry, this way enabling polarization dependent experiments, and an easy transfer from one beamline to another. An additional mirror system was established, that allows to deflect the beam downwards to also render investigations of liquid sample surfaces possible. The layout of the reflectometer setup is described, and some representative grazing incidence EXAFS measurements outlining the experimental capabilities of the system are presented.

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Publication Details

Journal
Journal of Physics Conference Series
Published
2025-05-01
DOI
https://doi.org/10.1088/1742-6596/3010/1/012067
Primary Topic
Climate change and permafrost
Type
article
Field-Weighted Citation Impact
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article

A new compact setup for in-situ grazing incidence X-ray experiments of solid and liquid samples

C. Schneider, Frederic Braun, Dirk Lützenkirchen−Hecht, Franz Eckelt et al.
Journal of Physics Conference Series
Climate change and permafrost
article

A new compact setup for in-situ grazing incidence X-ray experiments of solid and liquid samples

C. Schneider, Frederic Braun, Dirk Lützenkirchen−Hecht, Franz Eckelt, Lars F. Voss
article en

Abstract

Abstract A compact new X-ray reflectometer setup was realized, with a main design focus on mechanical stability and ruggedness, allowing in particular the change from a horizontal to a vertical scattering geometry, this way enabling polarization dependent experiments, and an easy transfer from one beamline to another. An additional mirror system was established, that allows to deflect the beam downwards to also render investigations of liquid sample surfaces possible. The layout of the reflectometer setup is described, and some representative grazing incidence EXAFS measurements outlining the experimental capabilities of the system are presented.

Journal of Physics Conference SeriesVol. 3010(1)
University of Wuppertal (DE)
Openalex Percentile: Top 83%
Climate change and permafrost
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