Solubility of hydrogen in liquid helium - development of a measurement apparatus

Abstract The solubility of hydrogen in liquid helium seems to be unknown. One potential explanation for this could be the exceedingly low solubility limit, making this phenomenon irrelevant for the vast majority of applications. In cryogenics, however, this effect is crucial. Traces of hydrogen in liquid helium and in the liquid helium supply systems result in a malfunction of liquid helium flow cryostats and throttle devices. The project HyLiqHe (granted by DFG) aims among other objectives to quantify the solubility limits by measurement. Two specialized disciplines must come together for success. On the one hand, cryogenic expertise is required, as the solubility process takes place at liquid helium temperature. On the other hand, the hydrogen contents to be quantified range from hundreds to tens of ppb (parts per billion). This stands for a challenge in analytics. An experimental setup is presented that allows the preparation, analysis and condensation of helium/hydrogen mixtures. The saturation pressure is adjustable and the presence of precipitated hydrogen particles can be detected. The current status of work and preliminary investigations are presented.

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Publication Details

Journal
IOP Conference Series Materials Science and Engineering
Published
2025-05-01
DOI
https://doi.org/10.1088/1757-899x/1327/1/012143
Primary Topic
Spacecraft and Cryogenic Technologies
Type
article
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article

Solubility of hydrogen in liquid helium - development of a measurement apparatus

Ch. Haberstroh, J Will
IOP Conference Series Materials Science and Engineering
Spacecraft and Cryogenic Technologies
article

Solubility of hydrogen in liquid helium - development of a measurement apparatus

Ch. Haberstroh, J Will
article en

Abstract

Abstract The solubility of hydrogen in liquid helium seems to be unknown. One potential explanation for this could be the exceedingly low solubility limit, making this phenomenon irrelevant for the vast majority of applications. In cryogenics, however, this effect is crucial. Traces of hydrogen in liquid helium and in the liquid helium supply systems result in a malfunction of liquid helium flow cryostats and throttle devices. The project HyLiqHe (granted by DFG) aims among other objectives to quantify the solubility limits by measurement. Two specialized disciplines must come together for success. On the one hand, cryogenic expertise is required, as the solubility process takes place at liquid helium temperature. On the other hand, the hydrogen contents to be quantified range from hundreds to tens of ppb (parts per billion). This stands for a challenge in analytics. An experimental setup is presented that allows the preparation, analysis and condensation of helium/hydrogen mixtures. The saturation pressure is adjustable and the presence of precipitated hydrogen particles can be detected. The current status of work and preliminary investigations are presented.

IOP Conference Series Materials Science and EngineeringVol. 1327(1)
Technische Universität Dresden (DE)
Openalex Percentile: Top 72%
Spacecraft and Cryogenic Technologies
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