Rapid Access to Enantiopure Protected (R)-Paraconyl Alcohol
Quan4ta4ve 1 H NMR of 1 (500 MHz, CDCl3, D1 = 60 seconds, NS = 4) Purity determined to be 92.5 wt% versus dimethylsulfone as internal standard as an average of two runs (only one shown here).Sample: 14.7 mg @ mw 113.10 dimethylsulfone: 22.9 mg @ 99.96% purity & mw 94.13 Sample Integral 1: 5.017 -4.784 ppm, value = 2.00 (2 nuclides)
Authors
- Haylie E. Hennigan
Publication Details
- Journal
- Organic Syntheses
- Published
- 2025-01-01
- DOI
- https://doi.org/10.15227/orgsyn.102.0251
- Citations
- 2
- Primary Topic
- Chemical Synthesis and Analysis
- Type
- article
- Field-Weighted Citation Impact
- 1.61