Synthesis, Optical Properties and Photocatalytic Testing of Sol–Gel TiO2-Fe2O3/PVP Nanopowders

In this study, TiO2-Fe2O3/polyvinylpyrrolidone (PVP) hybrids were prepared using the sol–gel method. The iron content in the synthesized samples was 10 and 20 wt%. The influence of PVP on the phase transformation, morphology and optical properties of the as-prepared hybrids was characterized by various physicochemical methods—XRD analysis, UV–Vis spectroscopy, IR spectroscopy and SEM. The obtained sol–gel powders were tested for photocatalytic activity against tetracycline hydrochloride in distilled water under ultraviolet and simulated solar light illumination. The obtained results were compared to commercial TiO2 P25 (Evonik). The investigated samples exhibited good photocatalytic efficiency for the degradation of tetracycline hydrochloride; however, better activity was demonstrated by the 90TiO2-10Fe2O3/PVP sample. The latter one displayed weak antibacterial action against E. coli ATCC 25922 in the presence of UVA light.

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Publication Details

Journal
Optics
Published
2025-05-26
DOI
https://doi.org/10.3390/opt6020022
Citations
1
Primary Topic
TiO2 Photocatalysis and Solar Cells
Type
article
Field-Weighted Citation Impact
0.36
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article

Synthesis, Optical Properties and Photocatalytic Testing of Sol–Gel TiO2-Fe2O3/PVP Nanopowders

Angelina Stoyanova, Martin Tsvetkov, Stefani Petrova, Yoanna Kostova et al.
1 citations
Optics
TiO2 Photocatalysis and Solar Cells
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article

Synthesis, Optical Properties and Photocatalytic Testing of Sol–Gel TiO2-Fe2O3/PVP Nanopowders

Angelina Stoyanova, Martin Tsvetkov, Stefani Petrova, Yoanna Kostova, Hristina Y. Hitkova, Albena Bachvarova-Nedelcheva, Polya Marinovska
article en
1 citations

Abstract

In this study, TiO2-Fe2O3/polyvinylpyrrolidone (PVP) hybrids were prepared using the sol–gel method. The iron content in the synthesized samples was 10 and 20 wt%. The influence of PVP on the phase transformation, morphology and optical properties of the as-prepared hybrids was characterized by various physicochemical methods—XRD analysis, UV–Vis spectroscopy, IR spectroscopy and SEM. The obtained sol–gel powders were tested for photocatalytic activity against tetracycline hydrochloride in distilled water under ultraviolet and simulated solar light illumination. The obtained results were compared to commercial TiO2 P25 (Evonik). The investigated samples exhibited good photocatalytic efficiency for the degradation of tetracycline hydrochloride; however, better activity was demonstrated by the 90TiO2-10Fe2O3/PVP sample. The latter one displayed weak antibacterial action against E. coli ATCC 25922 in the presence of UVA light.

OpticsVol. 6(2)
Bulgarian Academy of Sciences (BG), Institute of General and Inorganic Chemistry (BG), University of Chemical Technology and Metallurgy (BG), Institute of Metal Science, Equipment and Technologies (BG), Medical University Pleven (BG), Sofia University "St. Kliment Ohridski" (BG)
Openalex Percentile: Top 43%
TiO2 Photocatalysis and Solar Cells
0.36
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