Microstructure Evolution and Properties of ZrC–NbC System Titanium Matrix Composites Based on Experiments and ANSYS Simulations

The extreme environment of aerospace requires severe material properties, and in situ autogenous ZrC–NbC dual-phase reinforced titanium matrix composites have attracted much attention. In this study, TiC/Ti composites (TMC1–TMC4) with different NbC contents (0–9 wt%) were prepared and investigated in depth by various means and ANSYS simulations. The results show that the variation in NbC content significantly changes the TiC morphology from fine needles at 0 wt% to needles with a small amount of ellipsoidal grains at 3 wt%, to an ideal uniform distribution (mostly granular or nearly spherical) at 6 wt%, and to a large number of aggregates (dendritic or coarse rod-like) at 9 wt%. In terms of mechanical properties, the compressive strength and elongation firstly increased and then decreased, and reached the optimum at 6 wt% NbC, with the ultimate compressive strength as high as 1379.50 MPa, the compressive yield strength at 817.3 MPa, the compressive strain up to 38.73%, and typical ductile fracture characteristics; at 9 wt%, it transformed into a mixed fracture mode, with a decrease in performance. ZrC and NbC synergistically stabilize the microstructure, with the best synergistic effect at 6 wt% NbC, which effectively improves the overall performance and meets the requirements of aerospace applications. The simulation is highly compatible with the experiment and verifies the experiment; this helps to reveal the mechanism, provides guidance for the design of high-performance materials, and promotes the development of materials technology in the aerospace field.