Wire-based friction stir additive manufacturing of AZ31B magnesium alloy: Precipitate behavior and mechanical properties

• Wire-based friction stir additive manufacturing was utilized for magnesium alloy. • Continuous formation of defect-free components was prepared by solid-state process. • Refined grains and alternating texture structures along the BD were obtained. • The interfaces between Mg 17 Al 12 and matrix, as well as, Al 8 Mn 5 were coherent. • The alloy showed isotropy with 257 MPa/12 % in BD and 251 MPa/12 % in TD. Simultaneous achievement of defect-free formation and high mechanical performance in additive manufactured Mg alloys remains challenging, bottlenecked by flammability, porosities, and oxidation risks within the melting-solidifying process. Here, wire-based friction stir additive manufacturing (W-FSAM), sparked by continuous wire feeding, severe plastic deformation transport, and solid-state deposition, was exploited to achieve sound Mg components. Greatly refined grains were obtained by severe plastic deformation, with an average grain size of 3.79 µm. Al 8 Mn 5 precipitates underwent refinement and redistribution, while Mg 17 Al 12 precipitates experienced solid solution and precipitation behaviors. Lattice mismatch was 4.92 % when Mg 17 Al 12 precipitated on Al 8 Mn 5 . The strong flow-induced effect of the pin structure weakened the basal texture along the building direction, which was formed by the intense forging effect of W-FSAM tools. Alternating texture features coordinated the plastic deformation of slip and twinning, enabling superior ductility. Additionally, in-situ electron backscattered diffraction results revealed grain boundary sliding accommodated by grain rotation within the fine-grained structure. These unique microstructural features and precipitate behavior enhanced the overall mechanical properties, with an ultimate tensile strength of 257.3 ± 3.5 MPa and an elongation of 12.4 ± 0.3 % in building direction, and an ultimate tensile strength of 250.7 ± 2.0 MPa and an elongation of 12.2 ± 0.5 % in the traveling direction.

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Publication Details

Journal
Journal of Magnesium and Alloys
Published
2025-05-22
DOI
https://doi.org/10.1016/j.jma.2025.04.025
Citations
53
Primary Topic
Aluminum Alloys Composites Properties
Type
article
Field-Weighted Citation Impact
37.81
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article

Wire-based friction stir additive manufacturing of AZ31B magnesium alloy: Precipitate behavior and mechanical properties

Yuming Xie, Naijie Wang, Zeyu Zhang, Xiaotian Ma et al.
53 citations
Journal of Magnesium and Alloys
Aluminum Alloys Composites Properties
37.81
article

Wire-based friction stir additive manufacturing of AZ31B magnesium alloy: Precipitate behavior and mechanical properties

Yuming Xie, Naijie Wang, Zeyu Zhang, Xiaotian Ma, Xiangchen Meng, Wenjiang Dong, Jianing Dong, Yongxian Huang, Xiuwen Sun, Huijia Tian
article en
53 citations

Abstract

• Wire-based friction stir additive manufacturing was utilized for magnesium alloy. • Continuous formation of defect-free components was prepared by solid-state process. • Refined grains and alternating texture structures along the BD were obtained. • The interfaces between Mg 17 Al 12 and matrix, as well as, Al 8 Mn 5 were coherent. • The alloy showed isotropy with 257 MPa/12 % in BD and 251 MPa/12 % in TD. Simultaneous achievement of defect-free formation and high mechanical performance in additive manufactured Mg alloys remains challenging, bottlenecked by flammability, porosities, and oxidation risks within the melting-solidifying process. Here, wire-based friction stir additive manufacturing (W-FSAM), sparked by continuous wire feeding, severe plastic deformation transport, and solid-state deposition, was exploited to achieve sound Mg components. Greatly refined grains were obtained by severe plastic deformation, with an average grain size of 3.79 µm. Al 8 Mn 5 precipitates underwent refinement and redistribution, while Mg 17 Al 12 precipitates experienced solid solution and precipitation behaviors. Lattice mismatch was 4.92 % when Mg 17 Al 12 precipitated on Al 8 Mn 5 . The strong flow-induced effect of the pin structure weakened the basal texture along the building direction, which was formed by the intense forging effect of W-FSAM tools. Alternating texture features coordinated the plastic deformation of slip and twinning, enabling superior ductility. Additionally, in-situ electron backscattered diffraction results revealed grain boundary sliding accommodated by grain rotation within the fine-grained structure. These unique microstructural features and precipitate behavior enhanced the overall mechanical properties, with an ultimate tensile strength of 257.3 ± 3.5 MPa and an elongation of 12.4 ± 0.3 % in building direction, and an ultimate tensile strength of 250.7 ± 2.0 MPa and an elongation of 12.2 ± 0.5 % in the traveling direction.

Journal of Magnesium and AlloysVol. 15
Harbin Institute of Technology (CN)
Openalex Percentile: Top 0%
Aluminum Alloys Composites Properties
37.81
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