Formation of the <i>E</i>-isomer as an impurity in the optimized flow synthesis of a <i>Z</i>-α-thio-β-chloroacrylamide; <i>E</i>/<i>Z</i> photoisomerization in batch and flow, and solid state characterization of both isomers

The Z / E isomers of N -(4-methylphenyl)-3-chloro-2-(phenylthio)propenamide, the Z isomer being a valuable synthetic substrate, were photo-interconverted both in batch and in flow, and the detailed crystal chemistry of both isolated solids elucidated.

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Journal
Reaction Chemistry & Engineering
Published
2025-01-01
DOI
https://doi.org/10.1039/d5re00137d
Primary Topic
Innovative Microfluidic and Catalytic Techniques Innovation
Type
article
Field-Weighted Citation Impact
0.00

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article

Formation of the E-isomer as an impurity in the optimized flow synthesis of a Z-α-thio-β-chloroacrylamide; E/Z photoisomerization in batch and flow, and solid state characterization of both isomers

Anita R. Maguire, H.A. Moynihan, Olga C. Dennehy, Denis Lynch et al.
Reaction Chemistry & Engineering
Innovative Microfluidic and Catalytic Techniques Innovation
article

Formation of the E-isomer as an impurity in the optimized flow synthesis of a Z-α-thio-β-chloroacrylamide; E/Z photoisomerization in batch and flow, and solid state characterization of both isomers

Anita R. Maguire, H.A. Moynihan, Olga C. Dennehy, Denis Lynch, Simon E. Lawrence, U. B. Rao Khandavilli, Stuart G. Collins
article en

Abstract

The Z / E isomers of N -(4-methylphenyl)-3-chloro-2-(phenylthio)propenamide, the Z isomer being a valuable synthetic substrate, were photo-interconverted both in batch and in flow, and the detailed crystal chemistry of both isolated solids elucidated.

Reaction Chemistry & EngineeringVol. 10(8)
University College Cork (IE)
Science Foundation Ireland, European Regional Development Fund
Openalex Percentile: Top 90%
Innovative Microfluidic and Catalytic Techniques Innovation
DOIOpen Access PDFOpenAlex
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Formation of the <i>E</i>-isomer as an impurity in the optimized flow synthesis of a <i>Z</i>-α-thio-β-chloroacrylamide; <i>E</i>/<i>Z</i> photoisomerization in batch and flow, and solid state characterization of both isomers — Anita R. Maguire, H.A. Moynihan, et al. · Reaction Chemistry & Engineering (2025) | TGRS Research Map | TGRS