Enhanced crack stability in micro scale fracture testing via optimized bridge notches

In micro cantilever fracture, a bridge notch geometry with material ligaments at the notch ends helps to reduce focused ion beam artefacts near the notch root by arresting initial cracks and promoting fracture from sharp, natural cracks. Thus, it significantly reduces the statistical scatter in fracture toughness, a common but undesirable feature in micro fracture testing. Although this concept has been validated in simulations and experiments, systematic investigations into the optimal geometry remain lacking. In this study, we experimentally examine the influence of bridge width and notch depth on the fracture toughness of micro cantilevers, using single crystalline silicon as a model material. We found that samples with thinner material bridges and deeper notches exhibit crack arrest before failure, while those with thicker bridges do not show crack arrest instead exhibit apparent toughening. Cantilevers with an optimized bridge notch geometry for crack arrest exhibit a K IC of 1.09 ± 0.02 MPa m 0.5 , which agrees with previously reported fracture toughness for the Si (111) surface. Additionally, discrepancies between the bridge geometry in the experiment and the ideal structure resulted in a mismatch between the predicted and observed notch requirements for crack arrest. Our findings offer practical guidelines for designing bridge notch geometries to promote bridge failure, thus improving statistical analysis in micro fracture. • Bridge notch geometry for micro fracture experiments is optimized using silicon cantilevers fabricated by electron beam lithography and reactive ion etching. • Crack arrest is only observed in cantilevers with thin bridges and deep notches. • System dependent fracture toughness is measured for bridge notch geometries that did not show crack arrest. • A mismatch is identified between the simulated bridge notch geometry predicted for crack arrest and the experimental geometry.

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Publication Details

Journal
Materials Science and Engineering A
Published
2025-05-09
DOI
https://doi.org/10.1016/j.msea.2025.148479
Citations
4
Primary Topic
Ultrasonics and Acoustic Wave Propagation
Type
article
Field-Weighted Citation Impact
3.45
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Enhanced crack stability in micro scale fracture testing via optimized bridge notches

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Ultrasonics and Acoustic Wave Propagation
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article

Enhanced crack stability in micro scale fracture testing via optimized bridge notches

A. Muslija, Subin Lee, Eloho Anita Okotete, Jens Hohmann, Steffen Brinckmann, Christoph Kirchlechner, Manfred Kohl
article en
4 citations

Abstract

In micro cantilever fracture, a bridge notch geometry with material ligaments at the notch ends helps to reduce focused ion beam artefacts near the notch root by arresting initial cracks and promoting fracture from sharp, natural cracks. Thus, it significantly reduces the statistical scatter in fracture toughness, a common but undesirable feature in micro fracture testing. Although this concept has been validated in simulations and experiments, systematic investigations into the optimal geometry remain lacking. In this study, we experimentally examine the influence of bridge width and notch depth on the fracture toughness of micro cantilevers, using single crystalline silicon as a model material. We found that samples with thinner material bridges and deeper notches exhibit crack arrest before failure, while those with thicker bridges do not show crack arrest instead exhibit apparent toughening. Cantilevers with an optimized bridge notch geometry for crack arrest exhibit a K IC of 1.09 ± 0.02 MPa m 0.5 , which agrees with previously reported fracture toughness for the Si (111) surface. Additionally, discrepancies between the bridge geometry in the experiment and the ideal structure resulted in a mismatch between the predicted and observed notch requirements for crack arrest. Our findings offer practical guidelines for designing bridge notch geometries to promote bridge failure, thus improving statistical analysis in micro fracture. • Bridge notch geometry for micro fracture experiments is optimized using silicon cantilevers fabricated by electron beam lithography and reactive ion etching. • Crack arrest is only observed in cantilevers with thin bridges and deep notches. • System dependent fracture toughness is measured for bridge notch geometries that did not show crack arrest. • A mismatch is identified between the simulated bridge notch geometry predicted for crack arrest and the experimental geometry.

Materials Science and Engineering AVol. 939
Karlsruhe Institute of Technology (DE), FIZ Karlsruhe – Leibniz Institute for Information Infrastructure (DE), Forschungszentrum Jülich (DE), Kerntechnische Entsorgung Karlsruhe (Germany) (DE)
Affordable and clean energy
Openalex Percentile: Top 8%
Ultrasonics and Acoustic Wave Propagation
3.45
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