Optimal Conditions Linked to the Reducing Agent on the Role of Morphology of Silver Nanoparticles
Abstract This study optimizes silver nanoparticle synthesis using response surface methodology to predict particle size diameter. Factors including agitation frequency, flow, temperature, reducing agent concentration, and heating time were varied using citrate and borohydride separately. Particle size was measured via dynamic light scattering and morphology analyzed by transmission electron microscope. Regardless of the reducing agent, concentration most significantly influenced particle size. Interactions were also crucial. Sodium borohydride synthesis yielded small, narrowly distributed nanoparticles across various size ranges. The study demonstrates the production of nanometric particles suitable for diverse technological applications.
Authors
- Rita de Cássia Siqueira Curto Valle (ORCID: https://orcid.org/0000-0001-6614-788X)
- Ariovaldo Bolzan (ORCID: https://orcid.org/0000-0002-9303-9291)
- Cintia Marangoni (ORCID: https://orcid.org/0000-0003-2524-6501)
- Ricardo Antônio Francisco Machado (ORCID: https://orcid.org/0000-0003-1959-1456)
- el-Kazzaz Sa
- Angelo Oliveira Silva
Institutions
- Universidade Federal de Santa Catarina (BR)
Publication Details
- Journal
- Chemical Engineering & Technology
- Published
- 2025-05-05
- DOI
- https://doi.org/10.1002/ceat.70035
- Citations
- 2
- Primary Topic
- Gold and Silver Nanoparticles Synthesis and Applications
- Type
- article
- Field-Weighted Citation Impact
- 0.85
Funders
- Coordenação de Aperfeiçoamento de Pessoal de Nível Superior
- Conselho Nacional de Desenvolvimento Científico e Tecnológico
- Laboratório Central de Microscopia Eletrônica, Universidade Federal de Santa Catarina