Optimal Conditions Linked to the Reducing Agent on the Role of Morphology of Silver Nanoparticles

Abstract This study optimizes silver nanoparticle synthesis using response surface methodology to predict particle size diameter. Factors including agitation frequency, flow, temperature, reducing agent concentration, and heating time were varied using citrate and borohydride separately. Particle size was measured via dynamic light scattering and morphology analyzed by transmission electron microscope. Regardless of the reducing agent, concentration most significantly influenced particle size. Interactions were also crucial. Sodium borohydride synthesis yielded small, narrowly distributed nanoparticles across various size ranges. The study demonstrates the production of nanometric particles suitable for diverse technological applications.

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Publication Details

Journal
Chemical Engineering & Technology
Published
2025-05-05
DOI
https://doi.org/10.1002/ceat.70035
Citations
2
Primary Topic
Gold and Silver Nanoparticles Synthesis and Applications
Type
article
Field-Weighted Citation Impact
0.85

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article

Optimal Conditions Linked to the Reducing Agent on the Role of Morphology of Silver Nanoparticles

Rita de Cássia Siqueira Curto Valle, Ariovaldo Bolzan, Cintia Marangoni, Ricardo Antônio Francisco Machado et al.
2 citations
Chemical Engineering & Technology
Gold and Silver Nanoparticles Synthesis and Applications
0.85
article

Optimal Conditions Linked to the Reducing Agent on the Role of Morphology of Silver Nanoparticles

Rita de Cássia Siqueira Curto Valle, Ariovaldo Bolzan, Cintia Marangoni, Ricardo Antônio Francisco Machado, el-Kazzaz Sa, Angelo Oliveira Silva
article en
2 citations

Abstract

Abstract This study optimizes silver nanoparticle synthesis using response surface methodology to predict particle size diameter. Factors including agitation frequency, flow, temperature, reducing agent concentration, and heating time were varied using citrate and borohydride separately. Particle size was measured via dynamic light scattering and morphology analyzed by transmission electron microscope. Regardless of the reducing agent, concentration most significantly influenced particle size. Interactions were also crucial. Sodium borohydride synthesis yielded small, narrowly distributed nanoparticles across various size ranges. The study demonstrates the production of nanometric particles suitable for diverse technological applications.

Chemical Engineering & TechnologyVol. 48(6)
Universidade Federal de Santa Catarina (BR)
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior, Conselho Nacional de Desenvolvimento Científico e Tecnológico, Laboratório Central de Microscopia Eletrônica, Universidade Federal de Santa Catarina
Openalex Percentile: Top 29%
Gold and Silver Nanoparticles Synthesis and Applications
0.85
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