Methodological Basis for Reliable Evaluation of Air Void Structure Parameters Using the 2D Method

Frost resistance of pavement concrete is closely related to air void structure. Traditionally, such a structure is assessed by measuring chord lengths according to the guidelines provided in the PN-EN 480-11 standard. In recent years, increased attention has been given to analyzing pore diameters (2D) on the surface of concrete samples. The measurement procedure employed in the surface method should enable accurate identification of small pores formed by modern air-entraining admixtures. Researchers suggest only pores under 300 µm significantly impact frost resistance, raising the question of whether pores over 1000 µm should be considered in measurements. This study attempts to define the measurement frame parameters required to obtain satisfactory results. Additionally, a comparative analysis of air void structure parameters from 2D and 1D methods was conducted. Geometrical models of air voids distributed within cement paste using the Monte Carlo method based on air void structure data derived from real concrete were created. Analysis of these models demonstrated good agreement between the 2D and 1D results. It was concluded that satisfactory results require the analysis of either three measurement frames of 50 × 50 mm or four frames of 40 × 40 mm, with a resolution of at least 3 µm/px.

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Journal
Materials
Published
2025-05-02
DOI
https://doi.org/10.3390/ma18092095
Primary Topic
Concrete and Cement Materials Research
Type
article
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Methodological Basis for Reliable Evaluation of Air Void Structure Parameters Using the 2D Method

Jerzy Wawrzeńczyk, Henryk Kowalczyk
Materials
Concrete and Cement Materials Research
article

Methodological Basis for Reliable Evaluation of Air Void Structure Parameters Using the 2D Method

Jerzy Wawrzeńczyk, Henryk Kowalczyk
article en

Abstract

Frost resistance of pavement concrete is closely related to air void structure. Traditionally, such a structure is assessed by measuring chord lengths according to the guidelines provided in the PN-EN 480-11 standard. In recent years, increased attention has been given to analyzing pore diameters (2D) on the surface of concrete samples. The measurement procedure employed in the surface method should enable accurate identification of small pores formed by modern air-entraining admixtures. Researchers suggest only pores under 300 µm significantly impact frost resistance, raising the question of whether pores over 1000 µm should be considered in measurements. This study attempts to define the measurement frame parameters required to obtain satisfactory results. Additionally, a comparative analysis of air void structure parameters from 2D and 1D methods was conducted. Geometrical models of air voids distributed within cement paste using the Monte Carlo method based on air void structure data derived from real concrete were created. Analysis of these models demonstrated good agreement between the 2D and 1D results. It was concluded that satisfactory results require the analysis of either three measurement frames of 50 × 50 mm or four frames of 40 × 40 mm, with a resolution of at least 3 µm/px.

MaterialsVol. 18(9)
Kielce University of Technology (PL)
Sustainable cities and communities
Openalex Percentile: Top 90%
Concrete and Cement Materials Research
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Methodological Basis for Reliable Evaluation of Air Void Structure Parameters Using the 2D Method — Jerzy Wawrzeńczyk, Henryk Kowalczyk · Materials (2025) | TGRS Research Map | TGRS