Evaluation the TiO\(_2\) Phases by Raman Spectroscopy and X-ray Diffraction

TiO2 reported in all litterateurs with three phases anatase, rutile and brookite which variance in activities and most of chemical properties. The variance in properties represent one of the best strategy to enhance the activities. Thus in this work TiO2 were prepared with different crystal mixture from TiOSO4/H2O2 by change the values of pH for the solution (3, 8, 11 and 14). the synthesized TiO2 were characterized by Raman spectroscopy and X-ray diffraction and that shown different phases for the product. The results of analysis show that Anatase prefer acid solution which change to rutile and brookite or forming amorphous TiO2 with change the pH towards basic solution.

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Publication Details

Journal
International Research Journal of Pure and Applied Chemistry
Published
2025-04-26
DOI
https://doi.org/10.9734/irjpac/2025/v26i3917
Primary Topic
X-ray Diffraction in Crystallography
Type
article
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article

Evaluation the TiO\(_2\) Phases by Raman Spectroscopy and X-ray Diffraction

Abdulla M. Suhail, Wisam T. Hammadi, Azhar SH Al-Nasralla
International Research Journal of Pure and Applied Chemistry
X-ray Diffraction in Crystallography
article

Evaluation the TiO\(_2\) Phases by Raman Spectroscopy and X-ray Diffraction

Abdulla M. Suhail, Wisam T. Hammadi, Azhar SH Al-Nasralla
article en

Abstract

TiO2 reported in all litterateurs with three phases anatase, rutile and brookite which variance in activities and most of chemical properties. The variance in properties represent one of the best strategy to enhance the activities. Thus in this work TiO2 were prepared with different crystal mixture from TiOSO4/H2O2 by change the values of pH for the solution (3, 8, 11 and 14). the synthesized TiO2 were characterized by Raman spectroscopy and X-ray diffraction and that shown different phases for the product. The results of analysis show that Anatase prefer acid solution which change to rutile and brookite or forming amorphous TiO2 with change the pH towards basic solution.

International Research Journal of Pure and Applied ChemistryVol. 26(3)
Openalex Percentile: Top 94%
X-ray Diffraction in Crystallography
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