5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4<i>H</i>-pyran-3-carbonitrile dichlomethane hemisolvate

The title compound, 2C<sub>15</sub>H<sub>13</sub>FN<sub>2</sub>O<sub>2</sub>·CH<sub>2</sub>Cl<sub>2</sub>, crystallizes with two main mol-ecules in the asymmetric unit with a disordered di-chloro-methane solvent mol-ecule. The dihedral angles between the fluoro phenyl ring and 4<i>H</i>-pyran ring are 74.36 (15) and 80.69 (15)° in the two mol-ecules. In the crystal, N-H⋯N and N-H⋯O hydrogen bonds link the mol-ecules into a two-dimensional supra-molecular network propagating in the (100) plane.

Authors

Institutions

Publication Details

Journal
IUCrData
Published
2025-04-24
DOI
https://doi.org/10.1107/s2414314625003372
Citations
1
Primary Topic
Crystal structures of chemical compounds
Type
article
Field-Weighted Citation Impact
0.54

Funders

Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate

Eric M. Njogu, Sizwe J. Zamisa, Bernard Omondi, Carren Nyapola
1 citations
IUCrData
Crystal structures of chemical compounds
0.54
article

5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate

Eric M. Njogu, Sizwe J. Zamisa, Bernard Omondi, Carren Nyapola
article en
1 citations

Abstract

The title compound, 2C<sub>15</sub>H<sub>13</sub>FN<sub>2</sub>O<sub>2</sub>·CH<sub>2</sub>Cl<sub>2</sub>, crystallizes with two main mol-ecules in the asymmetric unit with a disordered di-chloro-methane solvent mol-ecule. The dihedral angles between the fluoro phenyl ring and 4<i>H</i>-pyran ring are 74.36 (15) and 80.69 (15)° in the two mol-ecules. In the crystal, N-H⋯N and N-H⋯O hydrogen bonds link the mol-ecules into a two-dimensional supra-molecular network propagating in the (100) plane.

IUCrDataVol. 10(4)
Multimedia University of Kenya (KE), University of KwaZulu-Natal (ZA)
Inyuvesi Yakwazulu-Natali
Clean water and sanitation
Openalex Percentile: Top 37%
Crystal structures of chemical compounds
0.54
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.