On the microstructural, mechanical, damping, wear properties of magnesium alloy AZ91-3 vol. % SiCP-3 vol. % fly ash hybrid composite and property correlation thereof

• AZ91 Mg alloy hybrid composite (3 vol. % SiC p and 3 vol. % fly ash particles) is fabricated using stir casting and hot extrusion. • Pair-wise property correlation map between grain size, density, mechanical, damping, and wear properties is developed. • Composite exhibited better mechanical properties in compression than tension. • Ductile and quasi-brittle failures are observed in unreinforced alloy and hybrid composite, respectively. • Composite showed improved wear, and damping capacity under time and temperature sweep modes. A combination of hard (SiC P ) and soft (fly ash) particulate reinforcements could be a strategy to enhance combination of multiple properties of Magnesium and its alloys which otherwise suffer from low stiffness, low wear resistance, and many other critical properties. However, at present a comprehensive and robust map correlating different properties in particle-reinforced composites is much lacking. In this work, an industrial grade AZ91 magnesium alloy reinforced with hard SiC and soft fly ash particles (with 3 vol. % each), has been prepared using stir casting followed by hot extrusion at 325 ∘ C with a ratio of 21.5. Microstructure of the hybrid composite was characterized using optical and scanning electron microscopes. The composite exhibited a reduction in average grain size from 13.6 to 7.1 µm, concomitantly an increase in Vickers hardness from 73 to 111 HV. The tension-compression yield asymmetry ratios of the unreinforced alloy and hybrid composite were 1.165 and 0.976, respectively indicating higher yield strength for the composite under compressive load. The composite exhibited 76% improvement in damping capacity under time sweep mode, and 28% improvement at 423 K under temperature sweep mode. The tribological characteristics of the composite under dry sliding conditions at sliding speeds and loads in the range of 0.5 to 1.5 m s -1 and 10 to 30 N, respectively showed higher wear resistance than the unreinforced alloy. The composite showed 23% improvement in sliding wear resistance at a load of 20 N and a speed of 1 m s -1 . Finally, efforts have been made to understand the influence of one property on the other by developing statistical property correlation maps from the properties obtained in this study and from the literature. These maps are expected to help in the design of hybrid Metal Matrix Composites for a variety of targeted applications in different sectors.

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Publication Details

Journal
Journal of Magnesium and Alloys
Published
2025-04-21
DOI
https://doi.org/10.1016/j.jma.2025.03.016
Citations
5
Primary Topic
Magnesium Alloys: Properties and Applications
Type
article
Field-Weighted Citation Impact
2.99

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article

On the microstructural, mechanical, damping, wear properties of magnesium alloy AZ91-3 vol. % SiCP-3 vol. % fly ash hybrid composite and property correlation thereof

Prince Gollapalli, A. R. Anilchandra, Millie Pant, M.K. Surappa
5 citations
Journal of Magnesium and Alloys
Magnesium Alloys: Properties and Applications
2.99
article

On the microstructural, mechanical, damping, wear properties of magnesium alloy AZ91-3 vol. % SiCP-3 vol. % fly ash hybrid composite and property correlation thereof

Prince Gollapalli, A. R. Anilchandra, Millie Pant, M.K. Surappa
article en
5 citations

Abstract

• AZ91 Mg alloy hybrid composite (3 vol. % SiC p and 3 vol. % fly ash particles) is fabricated using stir casting and hot extrusion. • Pair-wise property correlation map between grain size, density, mechanical, damping, and wear properties is developed. • Composite exhibited better mechanical properties in compression than tension. • Ductile and quasi-brittle failures are observed in unreinforced alloy and hybrid composite, respectively. • Composite showed improved wear, and damping capacity under time and temperature sweep modes. A combination of hard (SiC P ) and soft (fly ash) particulate reinforcements could be a strategy to enhance combination of multiple properties of Magnesium and its alloys which otherwise suffer from low stiffness, low wear resistance, and many other critical properties. However, at present a comprehensive and robust map correlating different properties in particle-reinforced composites is much lacking. In this work, an industrial grade AZ91 magnesium alloy reinforced with hard SiC and soft fly ash particles (with 3 vol. % each), has been prepared using stir casting followed by hot extrusion at 325 ∘ C with a ratio of 21.5. Microstructure of the hybrid composite was characterized using optical and scanning electron microscopes. The composite exhibited a reduction in average grain size from 13.6 to 7.1 µm, concomitantly an increase in Vickers hardness from 73 to 111 HV. The tension-compression yield asymmetry ratios of the unreinforced alloy and hybrid composite were 1.165 and 0.976, respectively indicating higher yield strength for the composite under compressive load. The composite exhibited 76% improvement in damping capacity under time sweep mode, and 28% improvement at 423 K under temperature sweep mode. The tribological characteristics of the composite under dry sliding conditions at sliding speeds and loads in the range of 0.5 to 1.5 m s -1 and 10 to 30 N, respectively showed higher wear resistance than the unreinforced alloy. The composite showed 23% improvement in sliding wear resistance at a load of 20 N and a speed of 1 m s -1 . Finally, efforts have been made to understand the influence of one property on the other by developing statistical property correlation maps from the properties obtained in this study and from the literature. These maps are expected to help in the design of hybrid Metal Matrix Composites for a variety of targeted applications in different sectors.

Journal of Magnesium and AlloysVol. 13(5)
Indian Institute of Technology Roorkee (IN), National Institute of Advanced Studies (IN), Bangalore University (IN), Indian Institute of Science Bangalore (IN)
Ministry of Education, India
Openalex Percentile: Top 10%
Magnesium Alloys: Properties and Applications
2.99
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