Optical and Structural Properties of 3R-MoS2 Synthesized at High Pressure

The rhombohedral (R3) phase of molybdenum disulfide (MoS2) is synthesized from elemental components at high temperatures and pressures. The crystal structure and lattice constants are determined by full-profile X-ray diffraction analysis of the synthesized powder. Scanning electron microscopy in combination with energy-dispersive X-ray microanalysis confirms the formation of layered crystals with the elemental composition of Mo and S in the ratio of 1 : 2. Luminescence spectra of the 3R-MoS2 bilayer transferred onto a SiO2/Si substrate demonstrate narrow emission lines characteristic of low-defect materials.

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Publication Details

Journal
Bulletin of the Lebedev Physics Institute
Published
2025-03-01
DOI
https://doi.org/10.3103/s1068335624602814
Citations
1
Primary Topic
2D Materials and Applications
Type
article
Field-Weighted Citation Impact
0.52
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article

Optical and Structural Properties of 3R-MoS2 Synthesized at High Pressure

Е. А. Екимов, I. I. Usmanov, P. V. Enkovich, С. Н. Николаев et al.
1 citations
Bulletin of the Lebedev Physics Institute
2D Materials and Applications
0.52
article

Optical and Structural Properties of 3R-MoS2 Synthesized at High Pressure

Е. А. Екимов, I. I. Usmanov, P. V. Enkovich, С. Н. Николаев, V. S. Krivobok, K.M. Kondrina
article en
1 citations

Abstract

The rhombohedral (R3) phase of molybdenum disulfide (MoS2) is synthesized from elemental components at high temperatures and pressures. The crystal structure and lattice constants are determined by full-profile X-ray diffraction analysis of the synthesized powder. Scanning electron microscopy in combination with energy-dispersive X-ray microanalysis confirms the formation of layered crystals with the elemental composition of Mo and S in the ratio of 1 : 2. Luminescence spectra of the 3R-MoS2 bilayer transferred onto a SiO2/Si substrate demonstrate narrow emission lines characteristic of low-defect materials.

Bulletin of the Lebedev Physics InstituteVol. 52(3)
P.N. Lebedev Physical Institute of the Russian Academy of Sciences (RU), Moscow Institute of Physics and Technology (RU), Moscow Power Engineering Institute (RU), Institute for High Pressure Physics (RU), Moscow Aviation Institute (RU)
Affordable and clean energy
Openalex Percentile: Top 40%
2D Materials and Applications
0.52
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Optical and Structural Properties of 3R-MoS2 Synthesized at High Pressure — Е. А. Екимов, I. I. Usmanov, et al. · Bulletin of the Lebedev Physics Institute (2025) | TGRS Research Map | TGRS