Improved Setup for Decolourization Experiments with Granular and Powdered Adsorbent Materials Using UV-VIS Flow-through Cells

Textile wastewater treatment poses global challenges due to complex and costly processes, particularly in the adsorption-based decolourization step. Existing experimental methodologies for adsorption suffer from inconsistencies, hindering comparability across studies. To address this, we developed a universal setup integrating conventional adsorption methods with pharmaceutical dissolution techniques. This approach provides continuous UV-VIS monitoring of adsorption processes without external filtration, which is suitable for both fine powders (∼microns) and granular particles (∼millimetres) and is applicable to both natural and synthetic adsorbents. Case studies conducted with powdered and granular adsorbents confirmed this method's robustness, reproducibility, and enhanced accuracy, allowing real-time, precise monitoring. Overall, this versatile approach significantly improves reliability in adsorption experiments, offering a broadly applicable solution for adsorption monitoring in wastewater treatment research.•A versatile setup combining adsorption methods with flow-through UV-VIS spectrometry.•Enables continuous monitoring of decolourization without the need for external filtration.•Applicable to a wide range of adsorbent materials, from fine powders to granulates.

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Publication Details

Journal
MethodsX
Published
2025-03-27
DOI
https://doi.org/10.1016/j.mex.2025.103289
Primary Topic
Water Quality Monitoring and Analysis
Type
article
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article

Improved Setup for Decolourization Experiments with Granular and Powdered Adsorbent Materials Using UV-VIS Flow-through Cells

Martin Behringer, Brigitte Helmreich, Alisa Machner, Harald Hilbig
MethodsX
Water Quality Monitoring and Analysis
article

Improved Setup for Decolourization Experiments with Granular and Powdered Adsorbent Materials Using UV-VIS Flow-through Cells

Martin Behringer, Brigitte Helmreich, Alisa Machner, Harald Hilbig
article en

Abstract

Textile wastewater treatment poses global challenges due to complex and costly processes, particularly in the adsorption-based decolourization step. Existing experimental methodologies for adsorption suffer from inconsistencies, hindering comparability across studies. To address this, we developed a universal setup integrating conventional adsorption methods with pharmaceutical dissolution techniques. This approach provides continuous UV-VIS monitoring of adsorption processes without external filtration, which is suitable for both fine powders (∼microns) and granular particles (∼millimetres) and is applicable to both natural and synthetic adsorbents. Case studies conducted with powdered and granular adsorbents confirmed this method's robustness, reproducibility, and enhanced accuracy, allowing real-time, precise monitoring. Overall, this versatile approach significantly improves reliability in adsorption experiments, offering a broadly applicable solution for adsorption monitoring in wastewater treatment research.•A versatile setup combining adsorption methods with flow-through UV-VIS spectrometry.•Enables continuous monitoring of decolourization without the need for external filtration.•Applicable to a wide range of adsorbent materials, from fine powders to granulates.

MethodsXVol. 14
Technical University of Munich (DE)
Openalex Percentile: Top 91%
Water Quality Monitoring and Analysis
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Improved Setup for Decolourization Experiments with Granular and Powdered Adsorbent Materials Using UV-VIS Flow-through Cells — Martin Behringer, Brigitte Helmreich, et al. · MethodsX (2025) | TGRS Research Map | TGRS