Unveiling anomalous strengthening and deformation mechanism evolution in a Mg-Gd-Y-Zr alloy under rate-temperature coupling effects

• Lower strain rates (10 s⁻¹ to 10⁻³ s⁻¹) increase peak stress but reduce ductility around 150 °C. • Strength anomaly at 150 °C arises from strain aging, precipitation, and dislocation structures. • High strain rates significantly postpone the occurrence of softening and twinning termination. • High strain rates increase recrystallization temperature, enhancing efficiency and homogeneity. While the deformation behavior of rare-earth magnesium alloys at high temperatures has been extensively studied, the deformation mechanisms under moderate-to-low temperatures and high strain rates remain insufficiently understood. To address this gap, hot compression tests were conducted on a Mg-11Gd-3Y-0.5Zr (wt.%) alloy over a temperature range of 150 °C–450 °C under strain rates of 10⁻³ s⁻¹ (low strain rate (LSR)) and 10 s⁻¹ (high strain rate (HSR)) to explore the strain rate-temperature coupling effects during hot deformation. The results revealed an anomalous increase in peak stress at 150 °C–250 °C as the strain rate decreased, attributed to the combined effects of nano-precipitates, dislocation cell structures, and serrated flow induced by dynamic strain aging. At higher temperatures, strain rate influences softening pathways: under HSR at 450 °C, the effect of twinning shifts from strengthening to facilitating dynamic recrystallization (DRX), resulting in substantial grain refinement (∼4 µm, 81% area fraction at a strain of 0.6). In contrast, at LSR, softening is dominated by dynamic recovery at 350 °C, with limited DRX (∼4 µm grains, 10% area fraction at a strain of 0.6) occurs at 400 °C. These findings clarify the dual role of twinning and its interaction with rate-temperature conditions, providing valuable insights into optimizing the hot processing of rare-earth magnesium alloys.

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Publication Details

Journal
Journal of Magnesium and Alloys
Published
2025-04-14
DOI
https://doi.org/10.1016/j.jma.2025.03.018
Citations
4
Primary Topic
Magnesium Alloys: Properties and Applications
Type
article
Field-Weighted Citation Impact
2.39

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article

Unveiling anomalous strengthening and deformation mechanism evolution in a Mg-Gd-Y-Zr alloy under rate-temperature coupling effects

Jing Li, Wen Chen, Xiuzhu Han
4 citations
Journal of Magnesium and Alloys
Magnesium Alloys: Properties and Applications
2.39
article

Unveiling anomalous strengthening and deformation mechanism evolution in a Mg-Gd-Y-Zr alloy under rate-temperature coupling effects

Jing Li, Wen Chen, Xiuzhu Han
article en
4 citations

Abstract

• Lower strain rates (10 s⁻¹ to 10⁻³ s⁻¹) increase peak stress but reduce ductility around 150 °C. • Strength anomaly at 150 °C arises from strain aging, precipitation, and dislocation structures. • High strain rates significantly postpone the occurrence of softening and twinning termination. • High strain rates increase recrystallization temperature, enhancing efficiency and homogeneity. While the deformation behavior of rare-earth magnesium alloys at high temperatures has been extensively studied, the deformation mechanisms under moderate-to-low temperatures and high strain rates remain insufficiently understood. To address this gap, hot compression tests were conducted on a Mg-11Gd-3Y-0.5Zr (wt.%) alloy over a temperature range of 150 °C–450 °C under strain rates of 10⁻³ s⁻¹ (low strain rate (LSR)) and 10 s⁻¹ (high strain rate (HSR)) to explore the strain rate-temperature coupling effects during hot deformation. The results revealed an anomalous increase in peak stress at 150 °C–250 °C as the strain rate decreased, attributed to the combined effects of nano-precipitates, dislocation cell structures, and serrated flow induced by dynamic strain aging. At higher temperatures, strain rate influences softening pathways: under HSR at 450 °C, the effect of twinning shifts from strengthening to facilitating dynamic recrystallization (DRX), resulting in substantial grain refinement (∼4 µm, 81% area fraction at a strain of 0.6). In contrast, at LSR, softening is dominated by dynamic recovery at 350 °C, with limited DRX (∼4 µm grains, 10% area fraction at a strain of 0.6) occurs at 400 °C. These findings clarify the dual role of twinning and its interaction with rate-temperature conditions, providing valuable insights into optimizing the hot processing of rare-earth magnesium alloys.

Journal of Magnesium and AlloysVol. 13(6)
North China Electric Power University (CN), China Academy of Space Technology (CN), University of Science and Technology Beijing (CN)
National Natural Science Foundation of China, China Postdoctoral Science Foundation, Fundamental Research Funds for the Central Universities
Climate action
Openalex Percentile: Top 12%
Magnesium Alloys: Properties and Applications
2.39
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