Fe3O4@SiO2-LY-C-D-Pd as a new, effective, and magnetically recoverable catalyst for the synthesis of 1H-tetrazoles and asymmetric biphenyls

This research project explored the synthesis and characterization of a newly developed C-D-Pd complex immobilized on Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>-LY, designed as a reusable magnetic catalyst. The heterogeneous nanocatalyst was thoroughly characterized using EDS, FTIR, XRD, XPS, TGA, SEM, VSM, and ICP techniques. The Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>-LY-C-D-Pd catalyst demonstrates exceptional performance in catalyzing C-C coupling reactions and <sup>1</sup>H-tetrazole derivatives, achieving high product yields. This catalyst offers several advantages, including eco-friendly reaction conditions, minimal catalyst usage, a simple experimental setup, the elimination of harmful organic solvents, reduced reaction times, and the ability to accommodate diverse substrates. Additionally, the nanocatalyst is easily separable from the reaction mixture and can be reused multiple times without losing stability or catalytic efficiency.

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Publication Details

Journal
Scientific Reports
Published
2025-04-15
DOI
https://doi.org/10.1038/s41598-025-95922-x
Citations
5
Primary Topic
Synthesis of Tetrazole Derivatives
Type
article
Field-Weighted Citation Impact
4.68

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article

Fe3O4@SiO2-LY-C-D-Pd as a new, effective, and magnetically recoverable catalyst for the synthesis of 1H-tetrazoles and asymmetric biphenyls

Hamidah Abu Bakar, Jayanti Makasana, Ojas Prakashbhai Doshi, Shelesh krishna saraswat et al.
5 citations
Scientific Reports
Synthesis of Tetrazole Derivatives
4.68
article

Fe3O4@SiO2-LY-C-D-Pd as a new, effective, and magnetically recoverable catalyst for the synthesis of 1H-tetrazoles and asymmetric biphenyls

Hamidah Abu Bakar, Jayanti Makasana, Ojas Prakashbhai Doshi, Shelesh krishna saraswat, V. Kavitha, Suhas Ballal, Ahmed M. Naglah, Lakshay Bareja, Munthar Kadhim Abosaoda, Pushpa Negi Bhakuni
article en
5 citations

Abstract

This research project explored the synthesis and characterization of a newly developed C-D-Pd complex immobilized on Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>-LY, designed as a reusable magnetic catalyst. The heterogeneous nanocatalyst was thoroughly characterized using EDS, FTIR, XRD, XPS, TGA, SEM, VSM, and ICP techniques. The Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>-LY-C-D-Pd catalyst demonstrates exceptional performance in catalyzing C-C coupling reactions and <sup>1</sup>H-tetrazole derivatives, achieving high product yields. This catalyst offers several advantages, including eco-friendly reaction conditions, minimal catalyst usage, a simple experimental setup, the elimination of harmful organic solvents, reduced reaction times, and the ability to accommodate diverse substrates. Additionally, the nanocatalyst is easily separable from the reaction mixture and can be reused multiple times without losing stability or catalytic efficiency.

Scientific ReportsVol. 15(1)
Jain University (IN), Management and Science University (MY), Long Island University (US), King Saud University (SA), Iraqi University (IQ), Marwadi University (IN), Sathyabama Institute of Science and Technology (IN), Graphic Era University (IN), Chitkara University (IN)
King Saud University
Responsible consumption and production
Openalex Percentile: Top 6%
Synthesis of Tetrazole Derivatives
4.68
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