FINDS: an ImageJ script for rapid non-matrix diffraction spot identification in selected area electron diffraction patterns

Phase characterization with selected area electron diffraction (SAED) represents a significant challenge when the pattern contains a substantial number of diffraction spots arranged in concentric but incomplete rings. This is a common situation when the crystallites are neither large enough to form a single crystal pattern nor sufficiently small and numerous to form continuous Debye-Scherrer rings. In such circumstances, it is often extremely difficult to distinguish between reflections belonging to a specific phase or to identify reflections that originate from secondary phases. To facilitate the process of phase identification for these kinds of multiphase samples, a macro script with the recursive acronym FINDS (FINDS Identifies Non-matrix Diffraction Spots) was developed on the ImageJ/FIJI platform. The program allows the user to mark diffraction spots of known phases by superimposed rings, making it easy to identify and address additional reflections between them. In addition to the full functionality of calculating and plotting the diffraction ring patterns of the known phases in different styles and colors, FINDS also provides tools for locating spot positions and determining the corresponding d -values of the reflections of interest. The effectiveness of this approach and of the developed program in assisting the process of phase identification with SAED patterns of multiphase samples is demonstrated by two representative examples. The macro code of FINDS is published under GNU General Public License v3.0 or later at https://doi.org/10.5281/zenodo.13748483 .

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Publication Details

Journal
Powder Diffraction
Published
2024-10-16
DOI
https://doi.org/10.1017/s0885715624000538
Citations
1
Primary Topic
Electron and X-Ray Spectroscopy Techniques
Type
article
Field-Weighted Citation Impact
0.18

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article

FINDS: an ImageJ script for rapid non-matrix diffraction spot identification in selected area electron diffraction patterns

Thomas E. Weirich
1 citations
Powder Diffraction
Electron and X-Ray Spectroscopy Techniques
0.18
article

FINDS: an ImageJ script for rapid non-matrix diffraction spot identification in selected area electron diffraction patterns

Thomas E. Weirich
article en
1 citations

Abstract

Phase characterization with selected area electron diffraction (SAED) represents a significant challenge when the pattern contains a substantial number of diffraction spots arranged in concentric but incomplete rings. This is a common situation when the crystallites are neither large enough to form a single crystal pattern nor sufficiently small and numerous to form continuous Debye-Scherrer rings. In such circumstances, it is often extremely difficult to distinguish between reflections belonging to a specific phase or to identify reflections that originate from secondary phases. To facilitate the process of phase identification for these kinds of multiphase samples, a macro script with the recursive acronym FINDS (FINDS Identifies Non-matrix Diffraction Spots) was developed on the ImageJ/FIJI platform. The program allows the user to mark diffraction spots of known phases by superimposed rings, making it easy to identify and address additional reflections between them. In addition to the full functionality of calculating and plotting the diffraction ring patterns of the known phases in different styles and colors, FINDS also provides tools for locating spot positions and determining the corresponding d -values of the reflections of interest. The effectiveness of this approach and of the developed program in assisting the process of phase identification with SAED patterns of multiphase samples is demonstrated by two representative examples. The macro code of FINDS is published under GNU General Public License v3.0 or later at https://doi.org/10.5281/zenodo.13748483 .

Powder DiffractionVol. 40(1)
RWTH Aachen University (DE)
Deutsche Forschungsgemeinschaft, RWTH Aachen University
Openalex Percentile: Top 49%
Electron and X-Ray Spectroscopy Techniques
0.18
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