EVALUATION OF THE EFFECT OF MECHANOSYNTHESIS PARAMETERS ON THE MORPHOLOGY OF A MAGNESIUM-BASED POWDER COMPOSITION

This article presents an analysis of the dependence of phase and morphological changes in the powder composition of the Mg-Ni-Ce system on the parameters of mechanical synthesis. During the mechanical synthesis process, it was found that, in addition to acceleration and duration parameters, the ratio of powder to milling balls has a significant influence on changes in the structural characteristics of the material. The results of the microscopic analysis showed that with a powderto-ball ratio of 1:10, the average particle size in the synthesized mixtures is 13.76 µm. At the same time, when applying a ratio of 1:30, the particle size decreases to 7.59 µm. It was established that magnesium is the primary phase in all samples. However, at a ratio of 1:30, the formation of the hexagonal crystal lattice of the MgNi phase and the emergence of the CeNi phase are identified.

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Publication Details

Journal
NNC RK Bulletin
Published
2025-04-01
DOI
https://doi.org/10.52676/1729-7885-2025-1-64-71
Citations
2
Primary Topic
Hydrogen Storage and Materials
Type
article
Field-Weighted Citation Impact
1.04
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article

EVALUATION OF THE EFFECT OF MECHANOSYNTHESIS PARAMETERS ON THE MORPHOLOGY OF A MAGNESIUM-BASED POWDER COMPOSITION

А. Zh. Miniyazov, Nuriya Mukhamedova, Zh. N. Ospanova, Ospan Oken et al.
2 citations
NNC RK Bulletin
Hydrogen Storage and Materials
1.04
article

EVALUATION OF THE EFFECT OF MECHANOSYNTHESIS PARAMETERS ON THE MORPHOLOGY OF A MAGNESIUM-BASED POWDER COMPOSITION

А. Zh. Miniyazov, Nuriya Mukhamedova, Zh. N. Ospanova, Ospan Oken, Karina Serikkyzy Shaikieva, Aisara Sabyrtayeva, T. D. Akhmedi
article en
2 citations

Abstract

This article presents an analysis of the dependence of phase and morphological changes in the powder composition of the Mg-Ni-Ce system on the parameters of mechanical synthesis. During the mechanical synthesis process, it was found that, in addition to acceleration and duration parameters, the ratio of powder to milling balls has a significant influence on changes in the structural characteristics of the material. The results of the microscopic analysis showed that with a powderto-ball ratio of 1:10, the average particle size in the synthesized mixtures is 13.76 µm. At the same time, when applying a ratio of 1:30, the particle size decreases to 7.59 µm. It was established that magnesium is the primary phase in all samples. However, at a ratio of 1:30, the formation of the hexagonal crystal lattice of the MgNi phase and the emergence of the CeNi phase are identified.

NNC RK Bulletin(1)
Institute of Atomic Energy (PL)
Openalex Percentile: Top 26%
Hydrogen Storage and Materials
1.04
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EVALUATION OF THE EFFECT OF MECHANOSYNTHESIS PARAMETERS ON THE MORPHOLOGY OF A MAGNESIUM-BASED POWDER COMPOSITION — А. Zh. Miniyazov, Nuriya Mukhamedova, et al. · NNC RK Bulletin (2025) | TGRS Research Map | TGRS