Insight into zero-valent iron at the nanoscale and its silica composites: Synthesis and characterization

Nanoscale zero-valent iron (nZVI) is thought to be the most effective remediation material for contaminated soil, especially when it comes to heavy metal pollutants. In the current high-industrial and technologically advanced period, water pollution has emerged as one of the most significant causes for concern. In this instance, silica was coated with zero-valent iron nanoparticles at 650 and 800 ℃. Ferric iron with various counter-ions, nitrate (FN) and chloride (FC), and sodium borohydride as a reducing agent were used to create nanoscale zero-valent iron in an ethanol medium with nitrogen ambient conditions. X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM) techniques were employed to describe the structures of the generated zero-valent iron nanoparticles. Further, we investigated the electrical properties and adsorption characteristics of dyes such as alizarin red in an aqueous medium. As a result, zero-valent nano iron (nZVI), a core-shell environmental functional material, has found extensive application in environmental cleanup. The knowledge in this work will be useful for nZVI-related future research and real-world applications.

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Publication Details

Journal
Characterization and Application of Nanomaterials
Published
2025-04-01
DOI
https://doi.org/10.24294/can10461
Primary Topic
Catalysis and Oxidation Reactions
Type
article
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article

Insight into zero-valent iron at the nanoscale and its silica composites: Synthesis and characterization

Ibrahim S. El-Hallag, E.H. El‐Mossalamy, A. A. Al-Owais
Characterization and Application of Nanomaterials
Catalysis and Oxidation Reactions
article

Insight into zero-valent iron at the nanoscale and its silica composites: Synthesis and characterization

Ibrahim S. El-Hallag, E.H. El‐Mossalamy, A. A. Al-Owais
article en

Abstract

Nanoscale zero-valent iron (nZVI) is thought to be the most effective remediation material for contaminated soil, especially when it comes to heavy metal pollutants. In the current high-industrial and technologically advanced period, water pollution has emerged as one of the most significant causes for concern. In this instance, silica was coated with zero-valent iron nanoparticles at 650 and 800 ℃. Ferric iron with various counter-ions, nitrate (FN) and chloride (FC), and sodium borohydride as a reducing agent were used to create nanoscale zero-valent iron in an ethanol medium with nitrogen ambient conditions. X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM) techniques were employed to describe the structures of the generated zero-valent iron nanoparticles. Further, we investigated the electrical properties and adsorption characteristics of dyes such as alizarin red in an aqueous medium. As a result, zero-valent nano iron (nZVI), a core-shell environmental functional material, has found extensive application in environmental cleanup. The knowledge in this work will be useful for nZVI-related future research and real-world applications.

Characterization and Application of NanomaterialsVol. 8(2)
Openalex Percentile: Top 97%
Catalysis and Oxidation Reactions
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