Low-temperature UHV scanning tunneling microscope double sample holder for <i>in situ</i> exchangeable clean room processed samples

A generalization of the double sample holder (DSH) concept is presented for an ultra-high vacuum (UHV) low-temperature (LT) multi-probe scanning tunneling microscope (STM). In UHV, the DSH is carrying, side-by-side, a reference metal sample [Au(111) single crystal for STM tip apex preparation] and an ancillary stand-alone small sample holder (for samples originating from a clean room) that can be mounted in situ in/out of the DSH plate. STM tip navigation on both sample surfaces is performed using a UHV scanning electron microscope positioned above the STM stage. For demonstration, clean room nanofabricated graphene nano-gears (diameter down to 25 nm) on a sapphire sample are characterized using STM. The STM tip apices are cleaned on the atomically precise and UHV cleaned Au(111) reference sample surface. Using our new DSH plate and in situ STM tip apex re-preparation on the reference metallic sample, we demonstrate how a clean room originating sample can be imaged at the atomic resolution using our LT-UHV 4-STM.

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Publication Details

Journal
Review of Scientific Instruments
Published
2025-04-01
DOI
https://doi.org/10.1063/5.0228294
Primary Topic
Surface and Thin Film Phenomena
Type
article
Field-Weighted Citation Impact
0.00

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article

Low-temperature UHV scanning tunneling microscope double sample holder for in situ exchangeable clean room processed samples

Piyush Kanti Sarkar, Umamahesh Thupakula, We-Hyo Soe, Jimmy Faria et al.
Review of Scientific Instruments
Surface and Thin Film Phenomena
article

Low-temperature UHV scanning tunneling microscope double sample holder for in situ exchangeable clean room processed samples

Piyush Kanti Sarkar, Umamahesh Thupakula, We-Hyo Soe, Jimmy Faria, Ayako Omura Okano, Makoto Sakurai, Christian Joachim
article en

Abstract

A generalization of the double sample holder (DSH) concept is presented for an ultra-high vacuum (UHV) low-temperature (LT) multi-probe scanning tunneling microscope (STM). In UHV, the DSH is carrying, side-by-side, a reference metal sample [Au(111) single crystal for STM tip apex preparation] and an ancillary stand-alone small sample holder (for samples originating from a clean room) that can be mounted in situ in/out of the DSH plate. STM tip navigation on both sample surfaces is performed using a UHV scanning electron microscope positioned above the STM stage. For demonstration, clean room nanofabricated graphene nano-gears (diameter down to 25 nm) on a sapphire sample are characterized using STM. The STM tip apices are cleaned on the atomically precise and UHV cleaned Au(111) reference sample surface. Using our new DSH plate and in situ STM tip apex re-preparation on the reference metallic sample, we demonstrate how a clean room originating sample can be imaged at the atomic resolution using our LT-UHV 4-STM.

Review of Scientific InstrumentsVol. 96(4)
Centre National de la Recherche Scientifique (FR), University of Tsukuba (JP), National Institute for Materials Science (JP), Tsukuba University of Technology (JP), Centre National pour la Recherche Scientifique et Technique (CNRST) (MA), Centre d’Élaboration de Matériaux et d’Études Structurales (FR)
European Commission, Horizon 2020 Framework Programme, HORIZON EUROPE European Innovation Council
Industry, innovation and infrastructure
Openalex Percentile: Top 95%
Surface and Thin Film Phenomena
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